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Flower-like nickel metal organic skeleton nano-material preparation method and application thereof

A metal-organic framework and nanomaterial technology, applied in the field of ascorbic acid sensor preparation, can solve the problems of affecting the measurement results, unfavorable rapid analysis, cumbersome steps, etc., and achieve the effect of rapid response, ideal electrochemical stability and low cost

Inactive Publication Date: 2017-07-04
YANGZHOU UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most require high experimental conditions and operating techniques, and some methods are cumbersome and not conducive to rapid analysis
In addition, some methods of analysis by means of color will also affect the results of the determination due to the color of the sample to be tested

Method used

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  • Flower-like nickel metal organic skeleton nano-material preparation method and application thereof
  • Flower-like nickel metal organic skeleton nano-material preparation method and application thereof
  • Flower-like nickel metal organic skeleton nano-material preparation method and application thereof

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Embodiment Construction

[0030] The present invention will be further described with examples below in conjunction with the accompanying drawings and specific embodiments, but is not limited thereto.

[0031] 1. Process for preparing flower-shaped nickel metal-organic framework nanomaterials:

[0032] Weigh 0.096g Ni(NO 3 ) 2 •6H 2 O and 0.166g terephthalic acid (C 8 h 6 o 4 ) was dissolved in dimethylformamide (DMF) to obtain a mixed solution I.

[0033] Accurately prepare 2 mL of 0.4 M NaOH aqueous solution, and then slowly drop into the mixed solution I to obtain the mixed solution II, which is stirred at room temperature for 1 hour, and then hydrothermally reacted at 100°C for 8 hours. The obtained light green precipitate was washed with DMF and ethanol three times and then dried to obtain a flower-shaped nickel metal-organic framework nanomaterial.

[0034] Above Ni(NO 3 ) 2 •6H 2 O can also use NiSO 4 •H 2 O or Ni(CH 3 COO) 2 • 4H 2 O alternative.

[0035] The above NaOH aqueous ...

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Abstract

The invention relates to a flower-like nickel metal organic skeleton nano-material preparation method and an application thereof, which belong to the technical field of production of an ascorbic acid sensor. The flower-like nickel metal organic skeleton nano-material is prepared by a simple hydrothermal method, the raw materials have the advantages of non toxin, environmental protection, and low cost, the technology is simple, operation is easily controlled, the method is suitable for continuous large-scale production, the preparation processes are environmentally friendly. The nano material has excellent electrochemistry response, wide linear scope, high sensitivity, good anti-interference capability and ideal electrochemical stability, and can be used for electrochemical sensing.

Description

technical field [0001] The invention belongs to the technical field of preparation of ascorbic acid sensors. Background technique [0002] Ascorbic acid is an essential vitamin and an antioxidant that improves the body's immunity and responsiveness. It is a naturally occurring organic compound with antioxidant properties. It is one of the important vitamins for maintaining normal physiological functions of the body. It is widely found in fresh fruits, juices and green leafy vegetables. It participates in a series of metabolism and redox reactions in the body, and also helps to synthesize intercellular substances such as collagen and mucopolysaccharides. It is also indispensable in the synthesis of adrenal cortex hormones and redox in the body. The lack of ascorbic acid in the human body will lead to scurvy Therefore, the quantitative analysis of ascorbic acid is of great significance in the fields of medicine and food. [0003] At present, the determination methods of asco...

Claims

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Application Information

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IPC IPC(8): G01N27/327B82Y40/00
CPCG01N27/3278B82Y40/00
Inventor 庞欢薛俞琪郑莎莎唐燚剑薛怀国
Owner YANGZHOU UNIV
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