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A kind of black light-absorbing quartz rod and preparation method thereof

A quartz rod and black technology, which is applied in the field of black light-absorbing quartz rod and its preparation, can solve the problems of poor heat resistance, small thermal expansion coefficient, and low softening point of transparent quartz rods, and achieve good coloring uniformity, strong pressure resistance, The effect of wide light absorption range

Active Publication Date: 2019-10-29
LIANYUNGANG HONGYANG QUARTZ PROD
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Problems solved by technology

[0002] Black light-absorbing quartz glass has the characteristics of small thermal expansion coefficient, high resistance to thermal ablation, high strength, high temperature resistance, rapid cooling resistance, excellent thermal performance, and resistance to laser radiation. It is not doped, and the heat resistance of transparent quartz rods is not good. Low softening point, no light absorption, can not work for a long time at 1250 ℃ high temperature

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  • A kind of black light-absorbing quartz rod and preparation method thereof

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Embodiment Construction

[0024] The specific technical solutions of the present invention are further described so that those skilled in the art can further understand the present invention, without limiting their rights.

[0025] A black light-absorbing quartz rod, with high-purity quartz sand as the basic weight part raw material, adopts SiO 2 The content is greater than 99.998%, the hydroxyl content is less than 5 ppm, and the high-purity quartz sand of 45 mesh to 145 mesh is equipped with a trace element additive accounting for 1% to 5% of the mass percentage of the high-purity quartz sand. The trace element additive is composed of the following weight Raw material composition of proportioning:

[0026] Cobalt trioxide Co 2 o 3 1.0~1.2

[0027] Manganese dioxide MnO 2 0.2~0.4

[0028] Potassium dichromate K 2 Cr 2 o 7 0.4~0.6

[0029] Barium oxide BaO 0.05~0.15

[0030] Calcium nitrate Ca (NO 3 ) 2 4H 2 O 0.5~0.7

[0031] Nickel oxide NiO 0.1~0.3

[0032] Neodymium oxide Nd 2 o ...

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Abstract

The invention relates to a black light-absorption quartz rod and a preparation method thereof. According to the black light-absorption quartz rod, high purity quartz sand is adopted as a base weight part raw material and is matched with 1.6-4.0% by weight of a trace element additive, the SiO2 content of the high purity quartz sand is more than 99.998%, the hydroxyl group content of the high purity quartz sand is less than 5 ppm, the particle size of the high purity quartz sand is 45-145 mesh, and the trace element additive comprises Co2O3, MnO2, K2Cr2O7, BaO, Ca(NO3)2.4H2O, NiO, Nd2O3, Al2O3, and Ce(NO3)3.6H2O. According to the present invention, the novel non-ablative black light-absorption quartz rod controlled and molded by using the quartz rod whole coloring preparation process has advantages of good whole coloring uniformity, good toughness, strong pressure resistance, high-temperature resistance, quenching resistance, rapid-heating resistance, laser radiation resistance and wide light absorption range, wherein the softening point achieves more than 1850 DEG C, the cut-off wavelength can achieve 8-12 [mu]m, the absorption peak can achieve 0.17, and the dual-beam infrared transmittance can achieve zero.

Description

technical field [0001] The invention relates to a preparation technology of a quartz rod, in particular to a black light-absorbing quartz rod and a preparation method thereof. Background technique [0002] Black light-absorbing quartz glass has the characteristics of small thermal expansion coefficient, high resistance to thermal ablation, high strength, high temperature resistance, rapid cooling resistance, excellent thermal performance, and resistance to laser radiation. It is not doped, and the heat resistance of transparent quartz rods is not good. Low softening point, no light absorption, can not work for a long time at 1250 ℃ high temperature. Contents of the invention [0003] The technical problem to be solved by the present invention is to propose a black light-absorbing quartz rod with large size of rod body, good overall coloring uniformity, good toughness and strong pressure resistance. [0004] The technical problem to be solved in the present invention is ac...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C3/06C03C6/00C03C4/02C03C4/08C03B20/00
CPCC03B20/00C03C1/00C03C3/06C03C4/02C03C4/082
Inventor 徐传龙徐源徐煜清
Owner LIANYUNGANG HONGYANG QUARTZ PROD
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