Method for preparing YAG-based transparent ceramics under Mg aid system
A technology of transparent ceramics and sintering aids, which is applied in the field of advanced ceramic preparation and can solve undeveloped problems
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[0030] One of the present invention provides a method for preparing yttrium aluminum garnet (Yttrium aluminum garnet) by vacuum sintering under a non-annealing mechanism using a small amount of Mg single additive system 3 Al 5 O 12 The method of YAG)-based transparent ceramics is characterized in that a small amount of Mg is used as a single sintering aid, and a single-step vacuum sintering method is used to prepare YAG transparent ceramics with good optical quality without post-annealing. The transparent ceramic components should meet the following (1) formula or (2) formula:
[0031] (Re x Y 1-x ) 3 Al 5 O 12 (1)
[0032] Y 3 (Cr y Al 1-y ) 5 O 12 (2)
[0033] In the formula, the value range of x is 0≤x≤0.6, the range of y is 0≤y≤0.05, and Re is one of Ce, Nd, Yb, Er, Ho, Dy, Pr, Tm, Sm, Eu or Tb . The addition amount of Mg is 0.003~0.018wt.% of the total mass of Y, Al, Cr or Y, Al, and Re raw material powder. The final prepared YAG transparent ceramic has a linear transmittan...
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