Manufacturing method for bamboo wood surface loaded nanometer titania material
A nano-titanium dioxide, surface-loaded technology, applied in chemical instruments and methods, manufacturing tools, separation methods, etc., can solve the problems of uneven distribution of titanium dioxide, easy agglomeration, complex operation, etc., to achieve easy operation, simple production process, photocatalysis The effect of degrading formaldehyde
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[0028] ③Preparation of bamboo-based nano-titanium dioxide composites
[0029] Bamboo treated with DBD cold plasma was soaked in sulfonated nano-TIO 2 In the aqueous solution, soak for 5-15min, and fully stir the nano-TIO when soaking 2 aqueous solution. After soaking, take out the bamboo, rinse off the free nano-TIO on the surface of the bamboo with water 2 The material is then put into an oven to dry, the drying temperature is 70-100°C, and the drying time should not be too long to avoid serious curling of the bamboo, which is 10-20min.
[0030] The dried bamboo is treated with cold plasma such as DBD again, and then soaked in nano-TIO 2 The aqueous solution is circulated in this way to prepare the bamboo-based nano-titanium dioxide composite material.
example
[0031] Example: a kind of manufacture method of bamboo base nano-titanium dioxide composite material, comprises the following steps:
[0032] ①Sulfonation treatment of nano-titanium dioxide
[0033] Nano titanium dioxide (TIO 2 ): Anatase type, purity 99.8%, hydrophilic and lipophilic type, nano-particles are about 25nm.
[0034] Poly(4-styrenesulfonic acid)ammonium salt solution: Poly(4-ammonium styrene-sulfonic acid)), alias pas, mass fraction is 30%, molecular weight Mw≈20000, soluble in water.
[0035] will TIO 2 Nanoparticles are dispersed in 5% pas solution, and the solution is ultrasonically dispersed in an ultrasonic oscillator with a power of 5KW for 2 hours, and then left for 8 hours to make the TIO 2 Nanoparticles are sufficiently combined with pas, so that TIO 2 The nanoparticles are negatively charged. Then the TIO 2 Nanoparticles are washed and separated (at least twice) by a high-speed centrifuge to remove negatively charged polymer macromolecules in the s...
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