Antioxidant grease, preparation method and application thereof
An anti-oxidation and oil technology, applied in the direction of food ingredients as antioxidants, edible oil/fat, application, etc., can solve the problems of inability to effectively enhance the oxidation stability of edible oils, unsafe raw materials, narrow application range, etc., to achieve enhanced edible oils Safety, inhibition of increase in total number of bacterial colonies, effect of enhanced oxidative stability
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Embodiment 1
[0025] Ferulic acid and walnut oil were uniformly mixed at a mass ratio of 1 g: 20 g, 0.30 g of immobilized Candida antarctica lipase was added, and reacted at 60° C. for 24 hours. Timing starts when the immobilized enzyme is added, and after the reaction is completed, the lipase and unreacted ferulic acid are separated by filtration to obtain anti-oxidative walnut oil. Accurately weigh 3g of the oil to be tested, and evaluate the oxidation stability of Rancimat oil at 110°C. From attached figure 1 A and figure 1 B It can be seen that the oxidation induction time of crude oil is 1.85h, and the oxidation induction time of antioxidant walnut oil is 4.16h, and the oxidation stability of antioxidant walnut oil is significantly enhanced.
Embodiment 2
[0027] p-Hydroxybenzoic acid and linseed oil were uniformly mixed at a mass ratio of 1g:15g, 0.5g of immobilized Thermomyces lanuginosus lipase was added, and reacted at 60°C for 24 hours. Timing starts when the immobilized enzyme is added, and after the reaction is completed, the lipase is separated from the unreacted linseed oil by filtration to obtain the anti-oxidative linseed oil. Accurately weigh 3g of the oil to be tested, and evaluate the oxidation stability of Rancimat oil at 110°C. The results showed that the oxidation induction time of crude oil was 0.14h, and that of antioxidative linseed oil was 1.76h, and the oxidation stability of antioxidative linseed oil was significantly enhanced.
Embodiment 3
[0029] Sesamol and fish oil were mixed evenly at a mass ratio of 1g:30g, 0.30g of immobilized Rhizomucor miehei lipase was added, and reacted at 60°C for 18 hours. The timing starts from the addition of the immobilized enzyme. After the reaction, the lipase is separated from the unreacted sesamol by filtration to obtain the antioxidant fish oil. The color difference of the obtained antioxidant fish oil is not large, and the fishy smell is greatly weakened compared with the unreacted fish oil. Accurately weigh 3g of the oil to be tested, and conduct the Rancimat oil oxidation stability evaluation at 100°C. The results showed that the oxidation induction time of crude oil was 0.28h, and that of antioxidant fish oil was 2.39h, and the oxidation stability of antioxidant fish oil was significantly enhanced.
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