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Hygienic insecticidal suspoemulsion and preparation method thereof

A suspoemulsion and hygienic technology, which is applied in the field of hygienic insecticidal compositions containing pyrethroids, can solve the problems of unsatisfactory quick-killing effect, poor retention activity, and slow contact killing effect of pests, etc., and achieves difficulty in flocculation or emulsion reversal , widely popularized and applied, with remarkable effect

Active Publication Date: 2017-11-24
江苏功成生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] For a long time, the formulations for preparing pyrethroid active ingredients into hygienic insecticides are relatively simple, mainly including emulsifiable concentrates, emulsions in water, microemulsions, etc. Agents, etc.; the former is an emulsion, although the quick-killing effect is better, but the retention activity is poor because it is easily absorbed by the contact surface. Good retention activity, but because it does not contain organic solvents, the contact killing effect on pests is slow, and the quick killing effect is not ideal
[0004] It is well known in the industry that pyrethroids are divided into knockdown agents and lethal agents. The knockdown agents can exert excellent rapid knockdown effects at low concentrations, but the lethal effect is poor, and the lethal agents have high lethal activity. , but at the same content, it has a poorer rapid knock-down effect than the knock-down agent; but generally speaking, the compatibility of the liquid preparation in the form of emulsion and suspension is not good. During the research, we found that by adding A small amount of specific knock-down agent is formulated into a specific compound of a large amount of specific suspension form lethal agent in the form of emulsion, on the one hand, the rapid knock-down effect of the knock-down agent can be fully exerted in the emulsion, and the suspension form can be used again on the other hand. Give full play to the long-term retention lethal effect

Method used

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  • Hygienic insecticidal suspoemulsion and preparation method thereof
  • Hygienic insecticidal suspoemulsion and preparation method thereof
  • Hygienic insecticidal suspoemulsion and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0057] Dissolve 1.5 g of D-trans-permethrin in 8.5 g of methyl oleate, add emulsifying dispersant (calcium dodecylbenzenesulfonate 1.0 g, phenethylphenol polyoxyethylene ether phosphate triethanolamine Salt 1.5g, fatty alcohol polyoxyethylene ether 1.0g) Stir well, add 1g polyacrylamide / polyethylene glycol diacrylate copolymer, the ratio of the two is 0.3:1.2, the molecular weight is about 5 million, add to water In the phase, add an appropriate amount of defoamer and antifreeze, and shear at a high speed to obtain 50g of water emulsion for subsequent use;

[0058] Beta-cypermethrin 8.5g, wetting and dispersing agent (fatty alcohol polyoxyethylene ether 1.0g, ethylene oxide propylene oxide block copolymer 2.0g, phenethylphenol polyoxyethylene ether phosphate triethanolamine salt 2.0g) Mix and shear with an appropriate amount of antifreeze, defoamer, thickener, antifreeze, preservative and water, and then sand mill 50g of suspension for 2.5 hours for later use;

[0059] Stir a...

Embodiment 2

[0061] Dissolve 2.0 g of chlorofluoromethrin in 9.0 g of diethyl adipate, add emulsifying dispersant (calcium dodecylbenzenesulfonate 0.5 g, block polyether phosphate triethanolamine salt 1.0 g, fatty alcohol Polyoxyethylene ether 1.5g) Stir well, add 2g of sodium acrylate / sodium acryloyl dimethyl taurate copolymer, the ratio of the two is 1.5:0.4, the molecular weight is about 8 million, add to the water phase, and then add Add an appropriate amount of defoamer and antifreeze, and shear at high speed to obtain 50g of water emulsion for later use;

[0062] Mix cis-cypermethrin 18.0g, wetting and dispersing agent (fatty alcohol polyoxyethylene ether 0.5g, ethylene oxide propylene oxide block copolymer 3.0g, block polyether phosphate triethanolamine salt 1.0g) and appropriate amount of antifreeze Agent, defoamer, thickener, antifreeze, preservative and water are mixed and sheared first, and then sand milled for 2.5 hours to prepare a 50g suspension;

[0063] Stir and mix the ab...

Embodiment 3

[0065] Dissolve 3.0 g of transfluthrin in 6.0 g of tributyl citrate, add emulsifying dispersant (ethylene oxide propylene oxide block copolymer 1.5 g, block polyether phosphate triethanolamine salt 1.5 g, Fatty alcohol polyoxyethylene ether 1.0g) Stir well, add 0.5g of isooctyl acrylate / dimethyl diallyl ammonium chloride binary copolymer, the dosage ratio of the two is 1:0.3, and the molecular weight is about 15 million. Add it to the water phase, then add an appropriate amount of defoamer and antifreeze, and shear at high speed to obtain 50g of water emulsion for later use;

[0066] Mix 12.0g of beta-cyfluthrin, wetting and dispersing agent (1.0g of fatty alcohol polyoxyethylene ether, 2.0g of ethylene oxide propylene oxide block copolymer, 2.0g of naphthalenesulfonate formaldehyde condensate) and appropriate amount of antifreeze, Defoamer, thickener, antifreeze, preservative and water are first mixed and sheared, and then 50g of the suspension is sanded for 2.5 hours for lat...

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Abstract

The invention relates to hygienic insecticidal suspoemulsion. The suspoemulsion comprises the following components calculated in percentage by weight: 0.1 to 10% of an active component A, 0.5 to 40% of a solvent, 1.0 to 10% of an emulsifying dispersant, 1 to 30% of an active component B, 1.0 to 10% of a wetting dispersant, 0.2 to 5% of an emulsifying stabilizer, 0.05 to 10% of a thickener, 1.0 to 10% of an antifreeze agent, 0.1 to 1.0% of a defoamer, 0.1 to 1.0% of a preservative, 0.1 to 5.0% of an acid-base regulator, and the balance of water; the active component A is knockout pyrethroid; the active component B is fatal pyrethroid; the emulsifying stabilizer is a ultra-high molecular weight copolymer of which the relative molecular weight is 1 to 20 million; in the suspoemulsion, the emulsifying dispersant and the wetting dispersant are optimized, especially the special emulsifying stabilizer is supplemented to solve the stability problem existing in a suspoemulsion system.

Description

technical field [0001] The invention relates to the field of hygienic insecticides, in particular to a hygienic insecticide composition containing pyrethroids and its application. Background technique [0002] Pyrethroid pesticides are a class of insecticides artificially synthesized by simulating natural pyrethrins. Due to their advantages such as broad insecticidal spectrum, good effect, low residue, and no accumulation effect, their application has become more and more common in the past 30 years. In addition to preventing and controlling agricultural pests, it has achieved quite satisfactory killing effects in controlling pests such as vegetable and fruit tree pests, public health mosquitoes, flies, cockroaches, and head lice. [0003] For a long time, the formulations for preparing pyrethroid active ingredients into hygienic insecticides are relatively simple, mainly including emulsifiable concentrates, emulsions in water, microemulsions, etc. Agents, etc.; the former ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N53/10A01N53/08A01N53/06A01N25/04A01P7/04
CPCA01N25/04A01N53/00A01N2300/00
Inventor 黄昌建姚志牛
Owner 江苏功成生物科技有限公司
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