The invention belongs to the technical field of
chemical synthesis, and particularly relates to a preparation method of tetrafluthrin. According to the method, 2, 3, 5, 6-tetrafluorobenzyl
alcohol and dichlorochrysanthemoyl
chloride are taken as raw materials, and the tetraflubenthrin is synthesized under a
solvent-free condition. According to the method, the
transfluthrin is synthesized by adopting a
solvent-free method, processes such as
desolvation and
solvent treatment are not involved, the operation is simple, and the
energy consumption is low; meanwhile, since no solvent is used for synthesis, the single-batch productivity is remarkably improved; in the synthesis process, a three-stage falling film
tower is adopted for water absorption to become a byproduct acid, the
wastewater amount is small, and the economical efficiency is high; the falling film
microstructure reactor is adopted, so that the production efficiency is high, the operation is simple, convenient and safe,
continuous production can be realized, and clean production is met.