A kind of aluminum strontium tungsten master alloy and preparation method thereof
A technology of aluminum-strontium master alloy and master alloy, which is applied in the field of aluminum-strontium-tungsten master alloy and its preparation, can solve the problems of increasing impurities, increasing process links, and excessive, so as to reduce porosity, improve mechanical properties, and obtain high rate effect
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Embodiment 1
[0029] Weigh 99g aluminum strontium master alloy, 1g WO 3 ; Take CaF with a mass ratio of 1:35:35:1 2 , NaCl, KCl, Na 3 AlF 6 A total of 10g was mixed to form a flux, and mixed with WO 3 Mix to form a mixed powder; ball mill the mixed powder under vacuum protection, the ball milling speed is 350rpm, the ball to material ratio is 10:1, and the ball milling time is 8h; the mixed powder after ball milling is preheated to 400°C for 30min, and the Al-10Sr intermediate The alloy is heated to 800°C in a resistance furnace to melt, and the preheated mixed powder is wrapped with aluminum foil and pressed into the melt, and treated by acoustic-magnetic coupling for 10 minutes; the ultrasonic power is 1KW, and the frequency is 10KHz; Put it in place for 5 minutes to remove the slag and take it out of the furnace for casting.
Embodiment 2
[0031] Weigh 90g Al-Sr master alloy, 10g WO 3 ; Take by weighing CaF with a mass ratio of 10:45:45:10 2 , NaCl, KCl, Na 3 AlF 6 A total of 20g was mixed to form a flux, and mixed with WO 3 Mix to form a mixed powder; ball mill the mixed powder under vacuum protection, the ball milling speed is 350rpm, the ball-to-material ratio is 10:1, and the ball milling time is 8h; the ball-milled mixed powder is preheated to 500°C for 120min, and the Al-10Sr intermediate The alloy is heated to 800°C in a resistance furnace to melt, and the preheated mixed powder is wrapped with aluminum foil and pressed into the melt, and treated by acoustic-magnetic coupling for 10 minutes; the ultrasonic power is 1KW, and the frequency is 10KHz; Set it for 10 minutes to remove the slag and take it out of the furnace for casting.
Embodiment 3
[0033] Weigh 95g aluminum strontium master alloy, 5g WO 3 ; Take by weighing the CaF that mass ratio is 3:38:38:3 2 , NaCl, KCl, Na 3 AlF 6 A total of 15g was mixed to form a flux, and mixed with WO 3 Mix to form a mixed powder; ball mill the above mixed powder under vacuum protection, the ball milling speed is 350rpm, the ball-to-material ratio is 10:1, and the ball milling time is 8h; the ball-milled mixed powder is preheated to 450°C for 90min, The master alloy is melted by heating to 800°C in a resistance furnace, and the preheated mixed powder is wrapped with aluminum foil and pressed into the melt, and treated by acoustic-magnetic coupling for 10 minutes; the ultrasonic power is 1KW, and the frequency is 10KHz; after the treatment is completed Stand still for 15 minutes, remove the slag and take it out of the furnace for casting.
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