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Method used for preparing light wool fabric from NMMO aqueous solution

An aqueous solution and lightweight technology, applied in physical treatment, animal fibers, textiles and papermaking, etc., can solve the problems of difficult control, reduction of wool fiber skin affinity, long process, etc., and achieve the effect of reducing damage

Inactive Publication Date: 2017-11-28
SOUTHWEST UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the adsorption method mainly uses the intermolecular van der Waals force and ionic bond force to make the nanoparticles adsorb to the surface of the wool fiber, and the washing fastness is low; the process of the sol-gel method and the layer-by-layer assembly method is long and difficult to control; The coating method is to use adhesives to bond nanoparticles to the surface of wool fibers, which reduces the skin affinity of wool fibers to the human body

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] (1) Dissolve 20g NMMO and 3g tricarboxyethylphosphine in 100ml ethanol / water (volume ratio 1:4);

[0016] (2) Add 0.5 g of hollow glass microspheres to the solution obtained in step (1), and stir vigorously to obtain a solution in which hollow glass microspheres are dispersed;

[0017] (3) padding the woolen fabric in the solution solution obtained in step (2) several times, and the excess rate is 80%;

[0018] (4) Irradiate the padded wool fabric under 100W microwave for 10min;

[0019] (5) Soak the irradiated wool fabric in 25% polyvinyl alcohol aqueous solution to solidify for 10 minutes, then wash and dry.

Embodiment 2

[0021] (1) Dissolve 10g NMMO and 1g tricarboxyethylphosphine in 100ml ethanol / water (1:4 by volume);

[0022] (2) Add 0.2 g of hollow glass microspheres to the solution obtained in step (1), and stir vigorously to obtain a solution in which hollow glass microspheres are dispersed;

[0023] (3) padding the woolen fabric in the solution solution obtained in step (2) several times, and the excess rate is 90%;

[0024] (4) Irradiate the padded wool fabric under 120W microwave for 7 minutes;

[0025] (5) Soak the irradiated wool fabric in 22% polyvinyl alcohol aqueous solution to solidify for 10 minutes, then wash and dry.

Embodiment 3

[0027] (1) Dissolve 40g NMMO and 3g tricarboxyethylphosphine in 100ml ethanol / water (volume ratio 1:4);

[0028] (2) Add 1.2 g of hollow glass microspheres to the solution obtained in step (1), and stir vigorously to obtain a solution in which hollow glass microspheres are dispersed;

[0029] (3) padding the woolen fabric in the solution obtained in step (2) several times, and the excess rate is 100%;

[0030] (4) Irradiate the padded wool fabric under microwave at 150°C for 5 minutes;

[0031] (5) Soak the irradiated wool fabric in 12% polyvinyl alcohol aqueous solution to solidify for 10 minutes, then wash and dry.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention provides a method used for preparing light wool fabric from NMMO aqueous solution. The method comprises following steps: 1, NMMO and tris(2-carboxyethyl)phosphine are dissolved in an ethanol / water (volume ratio 1:4) solution so as to obtain a mixed solution; 2, hollow glass bead is added into the mixed solution, and violent stirring is carried out so as to obtain a dissolving solution containing dispersed hollow glass beads; 3, wool fabric is subjected to dip padding in the dissolving solution for a plurality of times; 4, after dip padding, the wool fabric is subjected to microwave irradiation; 5, after microwave irradiation, the wool fabric is immersed in a polyvinyl alcohol aqueous solution for curing, and then water washing and drying are carried out. The method is simple and convenient; cost is low; damage on wool fabric is low; wool fiber surface performance is not changed; the fastness of the hollow glass beads on wool fabric is high; no adhesive is used in the preparation process; and the method is nontoxic.

Description

technical field [0001] The invention relates to a method for preparing functional fabrics, in particular to a method for preparing lightweight wool fabrics with NMMO aqueous solution. Background technique [0002] Functional fiber materials can be prepared by introducing nanoparticles into textile fibers. At present, there are many preparation methods for introducing nanoparticles into wool fibers, such as: adsorption method, sol-gel method, layer-by-layer assembly method, coating method and so on. However, the adsorption method mainly uses the intermolecular van der Waals force and ionic bond force to make the nanoparticles adsorb to the surface of the wool fiber, and the washing fastness is low; the process of the sol-gel method and the layer-by-layer assembly method is long and difficult to control; The coating method is to use adhesives to bond nanoparticles to the surface of wool fibers, which reduces the skin affinity of wool fibers to the human body. [0003] N-meth...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06M15/333D06M10/00D06M13/282D06M13/477D06M11/82D06M101/12
CPCD06M15/333D06M10/003D06M11/82D06M13/282D06M13/477D06M2101/12
Inventor 卢明刘一萍
Owner SOUTHWEST UNIVERSITY
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