A kind of construction concrete made of modified hydrotalcite synergistically foaming and its preparation method
A technology of concrete and modified water, which is applied in the field of material processing, can solve the problems of insufficient foam concrete strength, unstable foam effect, and limited use fields, etc., and achieve the effects of easy large-scale industrial production, stable properties, and increased strength
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Embodiment 1
[0026] (1) Graft modification of hydrotalcite: first, immerse 3 parts by weight of layered structure hydrotalcite with a particle size of 300 microns in 0.2mol / L nitric acid, heat the nitric acid to 80°C, react for 4 hours, filter and immerse into 2 parts by weight of acrylic acid, through the anion replacement process, the time of the anion replacement process is 5 hours, and the reaction temperature is 45 ° C, so that the acrylic acid intercalation enters the interlayer of hydrotalcite, and then the intercalated hydrotalcite is placed in 5 weight After mixing ammonia water, keep the temperature of the reaction environment not exceeding 60°C, stir continuously during the reaction, and the stirring speed is 15 rpm, and the hydrotalcite intercalated with ammonium acrylate is obtained through the reaction. After the polymerization reaction of ammonium acrylate, ammonium polyacrylate is completed. grafting reaction;
[0027] (2) Preparation of foam: mixing and stirring the modifi...
Embodiment 2
[0032] (1) Graft modification of hydrotalcite: First, immerse 10 parts by weight of layered structure hydrotalcite with a particle size of 60 microns in 1.3mol / L nitric acid, heat the nitric acid to 50°C, react for 1 hour, filter and immerse into 2.5 parts by weight of acrylic acid, through the anion replacement process, the time of the anion replacement process is 2.5 hours, the reaction temperature is 45 ° C, so that the acrylic acid is intercalated into the interlayer of hydrotalcite, and then the intercalated hydrotalcite is placed in 2 weight After parting ammonia water, keep the temperature of the reaction environment not exceeding 60°C, keep stirring during the reaction process, the stirring speed is 12 rpm, and react to obtain ammonium acrylate-intercalated hydrotalcite. After the polymerization reaction of ammonium acrylate, ammonium polyacrylate is completed. grafting reaction;
[0033] (2) Preparation of foam: Mix and stir the modified hydrotalcite, 10 parts by weig...
Embodiment 3
[0038] (1) Graft modification of hydrotalcite: first immerse 5 parts by weight of layered structure hydrotalcite with a particle size of 120 microns in 0.5mol / L nitric acid, heat the nitric acid to 60°C, react for 3 hours, filter and immerse into 4 parts by weight of acrylic acid, and through the anion replacement process, the time of the anion replacement process is 5 hours, and the reaction temperature is 30 ° C, so that the acrylic acid is intercalated into the interlayer of hydrotalcite, and then the intercalated hydrotalcite is placed in 5 weight After mixing ammonia water, keep the temperature of the reaction environment not exceeding 60°C, stir continuously during the reaction, and the stirring speed is 15 rpm, and the hydrotalcite intercalated with ammonium acrylate is obtained through the reaction. After the polymerization reaction of ammonium acrylate, ammonium polyacrylate is completed. grafting reaction;
[0039] (2) Foam preparation: Mix and stir the modified hydrot...
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Abstract
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