Preparation method of inonotus obliquus coarse extraction liquid and inonotus obliquus extraction liquid
A technology of Inonotus obliquus and crude extract, which is applied in the field of extract preparation, can solve problems such as difficulty in effectively preventing polysaccharide degradation, low polysaccharide extraction rate, and easy degradation of polysaccharide, and achieves prevention of degradation, high polysaccharide content, and improved The effect of extraction rate
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[0032] The invention provides a method for preparing the crude extract of Inonotus obliquus, comprising the following preparation steps:
[0033] S100, putting the Inonotus obliquus raw material and graphene into the container;
[0034] S200, crushing the Inonotus obliquus raw material and graphene in the container to form a mixture M1;
[0035] S300, using ultraviolet rays to irradiate the M1 in the container;
[0036] S400. After the ultraviolet treatment is stopped, the mixture M1 is extracted to obtain an extract L;
[0037] S500. Concentrating the obtained extract L to obtain a crude extract of Inonotus obliquus.
[0038] The use of ultraviolet rays can promote the breakage of Inonotus obliquus and the dissolution of intracellular polysaccharides. However, ultraviolet rays will also accelerate the degradation of polysaccharides, resulting in a decrease in the extraction rate of polysaccharides. And add graphene in the present invention, because the aperture of graphene...
Embodiment 1
[0059] A preparation method of Inonotus obliquus crude extract:
[0060] (1) 200kg of Inonotus obliquus and 10kg of graphene were put into a container at 1°C and pulverized to 50 mesh, and treated with ultraviolet light for 1 hour;
[0061] (2) Stop the ultraviolet irradiation treatment, place the above-mentioned Inonotus obliquus in a container whose inner wall is a non-metallic material, add 1000 kg of normal temperature water, extract for 2 hours, and then filter out the extract L1 and collect it.
[0062] (3) Add hot water at 92°C to the container in the previous step until the total mass of the remaining materials and water is 1000kg, keep the water temperature at 92±2°C, extract for 3 hours, and then filter out the extract L2 and collect it.
[0063] (4) Add hot water at 85°C to the container in the previous step until the total mass of the remaining materials and water is 1100kg, add 0.8kg of salt, stir well, keep the water temperature at 85±2°C, extract for 3 hours, an...
Embodiment 2
[0068] A preparation method of Inonotus obliquus crude extract:
[0069] (1) 500kg of Inonotus obliquus and 30kg of graphene were put into a container at 4°C and pulverized to 20 mesh, and treated with ultraviolet light for 1.5h;
[0070] (2) Stop the ultraviolet irradiation treatment, place the above-mentioned Inonotus obliquus in a container whose inner wall is a non-metallic material, add 2500 kg of normal temperature water, extract for 3 hours, and then filter out the extract L1 and collect it.
[0071] (3) Add hot water at 85°C to the container in the previous step until the total mass of the remaining materials and water is 2500kg, keep the water temperature at 85±2°C, extract for 2 hours, then filter out the extract L2 and collect.
[0072] (4) Add hot water at 75°C to the container in the previous step until the total mass of the remaining materials and water is 2500kg, add 0.5kg of salt, stir well, keep the water temperature at 75±2°C, extract for 2 hours, and then ex...
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