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Preparation method and application of fructus hippophae extract Maillard reaction type tobacco flavor

A Maillard reaction and tobacco flavoring technology, which is applied in the field of cigarette flavoring, can solve the problems of untested and different cigarette flavors, and achieve the effect of simple operation, low production cost, and improved aroma quality

Inactive Publication Date: 2017-12-22
CHINA TOBACCO SHANDONG IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Although it is disclosed in the prior art that seabuckthorn fruit extracts and amino acids undergo Maillard reaction to prepare tobacco spices, it is necessary to add concentrated solutions of spice extracts such as Fritillaria japonicus, Gynostemma pentaphylla, honeysuckle, loquat leaves and lilies and seabuckthorn extracts. Fruit extracts are used to prepare tobacco flavors through Maillard reaction to achieve the purpose of smoothing smoke and enriching the aftertaste of cigarettes. On the one hand, the safety of the combustion products of these raw materials added in the human body remains to be verified. On the other hand, these The Maillard reaction product mixed with substances is completely different from sea buckthorn fruit, and the improvement of cigarette smoking taste is also completely different

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] (1) After removing impurities from the dried seabuckthorn fruit, pulverize and pass through an 80-mesh sieve for subsequent use;

[0044] (2) After adding ethanol solvent to the above seabuckthorn powder, utilize a high-speed homogenizer to carry out homogenization treatment, obtain the seabuckthorn sample after homogenization treatment;

[0045] (3) Extracting and separating the homogenized seabuckthorn sample obtained in step (2) by microwave extraction technology to obtain seabuckthorn extract;

[0046] (4) After filtering and vacuum-concentrating the seabuckthorn extract obtained in step (3), the seabuckthorn extract is obtained.

[0047] (5) take by weighing a certain amount of seabuckthorn extract of step (4) gained and join in the container, then add the ammonia substance of 10% of seabuckthorn extract weight, stir; Amine substance is alanine, glutamic acid and A mixture of phenylalanine in a mass ratio of 2:3:1.

[0048] (6) Add the mixture obtained in step (5...

Embodiment 2

[0055] (1) After removing impurities from the dried seabuckthorn fruit, pulverize and pass through an 80-mesh sieve for subsequent use;

[0056] (2) After adding ethanol solvent to the above seabuckthorn powder, utilize a high-speed homogenizer to carry out homogenization treatment, obtain the seabuckthorn sample after homogenization treatment;

[0057] (3) Extracting and separating the homogenized seabuckthorn sample obtained in step (2) by microwave extraction technology to obtain seabuckthorn extract;

[0058] (4) After filtering and vacuum-concentrating the seabuckthorn extract obtained in step (3), the seabuckthorn extract is obtained.

[0059] (5) Weighing a certain amount of seabuckthorn extract obtained in step (4) into a container, then adding 20% ​​of the weight of the seabuckthorn extract and stirring; the ammonia substance is alanine.

[0060] (6) Add the mixture obtained in step (5) to the reactor, and adjust the pH value to 5 with an acidic or basic compound; th...

Embodiment 3

[0064] (1) After removing impurities from the dried seabuckthorn fruit, pulverize and pass through an 80-mesh sieve for subsequent use;

[0065] (2) After adding ethanol solvent to the above seabuckthorn powder, utilize a high-speed homogenizer to carry out homogenization treatment, obtain the seabuckthorn sample after homogenization treatment;

[0066] (3) Extracting and separating the homogenized seabuckthorn sample obtained in step (2) by microwave extraction technology to obtain seabuckthorn extract;

[0067] (4) After filtering and vacuum-concentrating the seabuckthorn extract obtained in step (3), the seabuckthorn extract is obtained.

[0068] (5) Weigh a certain amount of seabuckthorn extract obtained in step (4) and add it into a container, then add 5% of the seabuckthorn extract by weight, and stir; the ammonia substance is alanine.

[0069] (6) Add the mixture obtained through step (5) into the reactor, and adjust the pH value to 12 with an acidic or basic compound;...

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Abstract

The invention discloses a fructus hippophae extract Maillard reaction type tobacco flavor as well as a preparation method and an application thereof. The preparation method of the tobacco flavor comprises the steps as follows: 1) after impurities of dried fructus hippophae are removed, the fructus hippophae is crushed and sieved with a 80-mesh sieve for later use; 2) an organic solvent is added to fructus hippophae powder obtained in the step 1), extraction is performed, and a fructus hippophae extracting solution is obtained; 3) the fructus hippophae extracting solution obtained in the step 2) is filtered and concentrated, and a fructus hippophae extract is obtained; 4) the fructus hippophae extract and ammonia substances are subjected to a Maillard reaction to produce a reaction product; 5) a certain amount of glycerin is added to the reaction product obtained in the step 4), and the fructus hippophae extract Maillard reaction type tobacco flavor is obtained. The method is highly targeted, the extract has rich aroma, after the extract is applied to cigarettes, the cigarette aroma can be better improved, the aroma quantity can be increased, the oral smoothness can be improved, the aftertaste can be improved, and the application effect of significantly improving the smoking quality of cigarettes can be realized.

Description

technical field [0001] The invention specifically relates to a preparation method of seabuckthorn extract Maillard reaction type tobacco flavoring and its application in cigarette flavoring, belonging to the technical field of cigarette flavoring. Background technique [0002] Seabuckthorn is a deciduous shrub or small tree of the genus Echinaceae, also known as vinegar willow. It is mainly distributed in more than ten provinces including Northwest my country, North China, Northeast China and Southwest China. Sea buckthorn fruit is rich in various vitamins, organic acids, flavonoids and trace elements, and has high nutritional and medicinal value. my country has made some progress in the application research of seabuckthorn, which is mainly used in food, medicine, cosmetics and other aspects. [0003] At present, the vast majority of seabuckthorn extracts for tobacco are mainly prepared from seabuckthorn as raw materials through simple extraction, filtration, concentration...

Claims

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Application Information

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IPC IPC(8): C11B9/02A24B3/12
CPCA24B3/12C11B9/02C11B9/022C11B9/025
Inventor 郑宏伟苏海建马长峰岳勇王强孙强于国锋杨景全
Owner CHINA TOBACCO SHANDONG IND
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