LED epitaxial growth method used for improving internal quantum efficiency
A technology of internal quantum efficiency and epitaxial growth, which is applied in the field of LED epitaxial growth to improve internal quantum efficiency, can solve the problems of low internal quantum efficiency of electronic leakage current LED, etc., to improve internal quantum efficiency and optical power, improve effective barrier height, Effect of suppressing electron leakage current
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Embodiment 1
[0051] Such as figure 1 and figure 2 As shown, the LED epitaxial growth method for improving internal quantum efficiency described in this embodiment includes the following steps:
[0052] Step 101, using metal chemical vapor deposition method MOCVD, in 1000°C-1100°C H 2 Under the atmosphere, feed 100L / min-130L / min of H 2 , keep the reaction chamber pressure at 100mbar-300mbar, and process the sapphire substrate for 5min-10min.
[0053] Step 102 , growing a low-temperature buffer layer GaN, and etching the low-temperature buffer layer GaN to form an irregular island shape.
[0054] Step 103 , growing an undoped GaN layer.
[0055] Step 104 , growing a Si-doped N-type GaN layer.
[0056] Step 105, keep the reaction chamber pressure at 800mbar-950mbar, keep the temperature at 750°C-900°C, and feed NH with a flow rate of 50000sccm-55000sccm (sccm is milliliters per minute) 3 , 50sccm-70sccm TMGa, 90L / min-110L / min H 2 , 1200sccm-1400sccm TMAl and 1000sccm-1500sccmDMZn, gro...
Embodiment 2
[0065] This embodiment specifically describes the specific content of growing the LED epitaxial layer as a whole, such as image 3 and Figure 4 As shown, the LED epitaxial growth method for improving internal quantum efficiency described in this embodiment includes the following steps:
[0066] Step 201, processing the sapphire substrate: into the reaction chamber of the metal-organic chemical vapor deposition system with the substrate placed, H at 1000°C-1100°C 2 Under the atmosphere, feed 100L / min-130L / min of H 2 , keep the reaction chamber pressure at 100mbar-300mbar, and process the sapphire substrate for 5min-10min.
[0067] Step 202, growing low-temperature buffer layer GaN: lower the temperature to 500°C-600°C, keep the reaction chamber pressure at 300mbar-600mbar, and feed NH with a flow rate of 10000sccm-20000sccm 3 , 50sccm-100sccm TMGa and 100L / min-130L / min H 2 , grow a low-temperature buffer layer GaN with a thickness of 20nm-40nm on a sapphire substrate.
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Embodiment 3
[0081] A conventional LED epitaxial growth method is provided below as a comparative example of the present invention.
[0082] Such as Figure 5 and Figure 6 As shown, the conventional LED epitaxial growth method includes the following steps:
[0083] Step 301, processing the sapphire substrate: Into the reaction chamber of the metal-organic chemical vapor deposition system with the substrate placed, H at 1000°C-1100°C 2 Under the atmosphere, feed 100L / min-130L / min of H 2 , keep the reaction chamber pressure at 100mbar-300mbar, and process the sapphire substrate for 5min-10min.
[0084] Step 302, grow low-temperature buffer layer GaN: lower the temperature to 500°C-600°C, keep the reaction chamber pressure at 300mbar-600mbar, and feed NH with a flow rate of 10000sccm-20000sccm 3 , 50sccm-100sccm TMGa and 100L / min-130L / min H 2 , grow a low-temperature buffer layer GaN with a thickness of 20nm-40nm on a sapphire substrate.
[0085] Raise the temperature to 1000°C-1100°C,...
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