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Production method of ink wax

A production method and ink technology, which are applied in the directions of ink, petroleum wax recycling, petroleum wax refining, etc., can solve the problems of low product yield, long production cycle, and inability to produce ink wax products.

Active Publication Date: 2020-04-14
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0014] The sweating process is an intermittent operation, and the product yield is low and the production cycle is long. However, the sweating process has the advantages of less investment, simple production process, low operating cost, safe production process, energy saving and no pollution to the environment. At present, there are still some Manufacturers are using this method to produce soap wax products
[0015] Over the years, the sweating method has been developed in terms of production equipment and technology, such as CN89214332 (vertical square multi-section sweating tank), CN94223980.6 (dish-type sweating device), CN98233254.8 (paraffin sweating tank), CN200920033500. X (new paraffin sweating tank), CN201210508905.0 (a high-efficiency paraffin sweating device), CN201320127680.4 (tubular paraffin deoiling device), etc., have made improvements in sweating production equipment; CN91206202 (a high-efficiency paraffin sweating tank ) Improvements have been made in the sweating process, but these improvements still cannot produce wax products for inks with a melting point of about 70 °C

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0079] This embodiment includes: (1) hydrogenation, (2) distillation, (3) emulsification, (4) sweating four parts.

[0080] (1) Hydrogenation

[0081] Same as Comparative Example 1.

[0082] (2) Distillation

[0083] Same as Comparative Example 1.

[0084] (3) Emulsification

[0085] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.

[0086] (A1) Oil phase material preparation

[0087] Take 80.0Kg of the 470℃~500℃ fraction prepared by (2) partial distillation, heat to 90℃ and melt, add 1.0Kg of sorbitan monostearate, 0.5Kg of diethylene glycol fatty acid ester, tetraethylene glycol Monostearate 1.5Kg, stir evenly.

[0088] (A2) Preparation of aqueous phase materials

[0089] 17.0 Kg of water was heated to 95°C.

[0090] (A3) Emulsion preparation

[0091] Stir the oil phase material prepared in (A1) at a speed of 500r / min, and slowly add the water phase material prepared in (A2) into th...

Embodiment 2

[0105] This embodiment includes: (1) hydrogenation, (2) distillation, (3) emulsification, (4) sweating four parts.

[0106] (1) Hydrogenation

[0107] Same as Comparative Example 1.

[0108] (2) Distillation

[0109] Same as Comparative Example 1.

[0110] (3) Emulsification

[0111] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.

[0112] (A1) Oil phase material preparation

[0113] Take 80.0Kg of the 470℃~500℃ fraction prepared by (2) partial distillation, heat to 90℃ and melt, add 1.5Kg of sorbitan monooleate, 1.0Kg of diethylene glycol monolaurate, lauryl Trimethylammonium chloride 0.5Kg, stir evenly.

[0114] (A2) Preparation of aqueous phase materials

[0115] 1.5Kg of KCl was dissolved in 15.5Kg of water and heated to 95°C.

[0116] (A3) Emulsion preparation

[0117] Stir the oil phase material prepared in (A1) at a speed of 700r / min, and slowly add the water phase material pr...

Embodiment 3

[0122] This embodiment includes: (1) hydrogenation, (2) distillation, (3) emulsification, (4) sweating four parts.

[0123] (1) Hydrogenation

[0124] With embodiment 1.

[0125] (2) Distillation

[0126] With embodiment 1.

[0127] (3) Emulsification

[0128] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.

[0129] (A1) Oil phase material preparation

[0130] Take 80.0Kg of the 470°C-500°C fraction prepared by (2) partial distillation, heat to 90°C and melt, add 1.5Kg of diethylene glycol fatty acid ester, 1.2Kg of sorbitan monopalmitate, oleamide carboxylic acid Sodium 0.3Kg, stir evenly.

[0131] (A2) Preparation of aqueous phase materials

[0132] 2.0 Kg of NaCl was dissolved in 15.0 Kg of water and heated to 95°C.

[0133] (A3) Emulsion preparation

[0134] Stir the oil phase material prepared in (A1) at a speed of 300r / min, and slowly add the water phase material prepared in (A...

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Abstract

The invention discloses a method for preparing ink wax. The method comprises carrying out hydro-conversion on an F-T synthesis product as a raw material under action of a catalyst, carrying out distillation on the hydrogenation product to obtain a component as a sweating raw material for a distillation range and carrying out emulsification and sweating to obtain a desired product. Based on the ordinary sweating method, airflows pass through a wax layer and carry away a liquid component in the sweating process so that a solid component and the liquid component are forcibly separated, and preferably, the sweating raw material and water or a salt solution are emulsified so that the liquid component can be fast discharged. The method has the advantages of low equipment investment, simple production process, low operation cost, safety, energy saving and no solvent pollution. The product has a narrow melting range and can be used as ink wax.

Description

technical field [0001] The invention belongs to the technical field of special wax production, and in particular relates to a production method of ink wax, especially a production method of wax used for hot-melt ink. Background technique [0002] Ink is an important material for printing. It expresses patterns and characters on the substrate through printing. Inks are widely used in various printings such as books, periodicals, packaging and decoration, architectural decoration and electronic circuit boards. With the increase of social demand, the variety and output of ink have also expanded and increased accordingly. [0003] Hot melt inks, or phase change inks or coldset inks, are solid at ambient temperatures and liquid at the higher temperatures at which inkjet printing devices operate. When the inkjet printing device is in operation, liquid ink droplets are ejected, and when the ink droplets directly or indirectly contact the surface of the recording substrate, they a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D11/12C10G73/36C10G73/42C10G73/44
CPCC09D11/12C10G73/36C10G73/42C10G73/44
Inventor 毕文卓孙剑锋袁平飞何凤友张志银赵永鹤
Owner CHINA PETROLEUM & CHEM CORP