Production method of ink wax
A production method and ink technology, which are applied in the directions of ink, petroleum wax recycling, petroleum wax refining, etc., can solve the problems of low product yield, long production cycle, and inability to produce ink wax products.
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Examples
Embodiment 1
[0079] This embodiment includes: (1) hydrogenation, (2) distillation, (3) emulsification, (4) sweating four parts.
[0080] (1) Hydrogenation
[0081] Same as Comparative Example 1.
[0082] (2) Distillation
[0083] Same as Comparative Example 1.
[0084] (3) Emulsification
[0085] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0086] (A1) Oil phase material preparation
[0087] Take 80.0Kg of the 470℃~500℃ fraction prepared by (2) partial distillation, heat to 90℃ and melt, add 1.0Kg of sorbitan monostearate, 0.5Kg of diethylene glycol fatty acid ester, tetraethylene glycol Monostearate 1.5Kg, stir evenly.
[0088] (A2) Preparation of aqueous phase materials
[0089] 17.0 Kg of water was heated to 95°C.
[0090] (A3) Emulsion preparation
[0091] Stir the oil phase material prepared in (A1) at a speed of 500r / min, and slowly add the water phase material prepared in (A2) into th...
Embodiment 2
[0105] This embodiment includes: (1) hydrogenation, (2) distillation, (3) emulsification, (4) sweating four parts.
[0106] (1) Hydrogenation
[0107] Same as Comparative Example 1.
[0108] (2) Distillation
[0109] Same as Comparative Example 1.
[0110] (3) Emulsification
[0111] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0112] (A1) Oil phase material preparation
[0113] Take 80.0Kg of the 470℃~500℃ fraction prepared by (2) partial distillation, heat to 90℃ and melt, add 1.5Kg of sorbitan monooleate, 1.0Kg of diethylene glycol monolaurate, lauryl Trimethylammonium chloride 0.5Kg, stir evenly.
[0114] (A2) Preparation of aqueous phase materials
[0115] 1.5Kg of KCl was dissolved in 15.5Kg of water and heated to 95°C.
[0116] (A3) Emulsion preparation
[0117] Stir the oil phase material prepared in (A1) at a speed of 700r / min, and slowly add the water phase material pr...
Embodiment 3
[0122] This embodiment includes: (1) hydrogenation, (2) distillation, (3) emulsification, (4) sweating four parts.
[0123] (1) Hydrogenation
[0124] With embodiment 1.
[0125] (2) Distillation
[0126] With embodiment 1.
[0127] (3) Emulsification
[0128] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0129] (A1) Oil phase material preparation
[0130] Take 80.0Kg of the 470°C-500°C fraction prepared by (2) partial distillation, heat to 90°C and melt, add 1.5Kg of diethylene glycol fatty acid ester, 1.2Kg of sorbitan monopalmitate, oleamide carboxylic acid Sodium 0.3Kg, stir evenly.
[0131] (A2) Preparation of aqueous phase materials
[0132] 2.0 Kg of NaCl was dissolved in 15.0 Kg of water and heated to 95°C.
[0133] (A3) Emulsion preparation
[0134] Stir the oil phase material prepared in (A1) at a speed of 300r / min, and slowly add the water phase material prepared in (A...
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Abstract
Description
Claims
Application Information
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