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A kind of preparation method of glazing wax

A wax layer and raw material technology, applied in chemical instruments and methods, polishing compositions, petroleum wax recycling, etc., can solve the problems of low production cycle, long production cycle, and inability to produce wax products.

Active Publication Date: 2020-04-10
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the ordinary sweating process produces soap wax and low melting point paraffin wax at 40°C to 60°C, the solid component (wax with a higher melting point) and the liquid component (wax with a lower melting point) in the sweating process are two types of components. They are in two phases of solid and liquid respectively, but it is difficult to completely separate them
In order to make the final product meet the requirements, the method of prolonging the sweating time (reducing the heating rate) and increasing the sweating termination temperature is usually adopted, but this will lead to a long production cycle and a decrease in product yield; tests have shown that the common sweating process produces products with a melting point above 70°C. For wax products, the carbon distribution width and n-alkane content on the wax in the later stage of sweating have nothing to do with the yield, that is, the carbon distribution width on the wax does not decrease with the decrease of yield, and the n-alkane content does not increase with the decrease of yield, so So far, there is no report on the production of wax products with a melting point of about 70°C by sweating process
[0016] Compared with solvent separation, the sweating process is an intermittent operation, and the product yield is lower and the production cycle is longer, but the sweating process has the advantages of less investment, simple production process, low operating cost, safe production process, energy saving and no pollution to the environment, etc. Advantages, some manufacturers are still using this method to produce soap wax products
[0017] Over the years, the sweating method has been developed in terms of equipment and technology, such as CN89214332 (vertical square multi-segment partition sweating tank), CN94223980.6 (dish-type sweating device), CN98233254.8 (paraffin wax sweating tank), CN200920033500.X (New paraffin sweating tank), CN201210508905.0 (a high-efficiency paraffin sweating device), CN201320127680.4 (tubular paraffin deoiling device), etc., improved sweating equipment; CN91206202 (a high-efficiency paraffin sweating tank) in Improvements have been made in the sweating process, but these improvements still cannot produce wax products with a melting point above 70°C

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0053] This embodiment includes: (1) sweating and (2) emulsification.

[0054] (1) Sweating: Including (1) preparation, (2) cooling - high temperature constant temperature - cooling - low temperature constant temperature crystallization, (3) heating - constant temperature sweating, (4) refining four steps.

[0055] (1) Preparation

[0056] Connect the sealing system of the sweating dish with the pressurized buffer tank and the compressor; install the decompression buffer tank and connect the vacuum pump at the lower part of the sweating dish; connect the jacket of the sweating dish and the movable coil with the circulation system, and fix the coil in the On the sweating dish; use heat transfer oil as the heating medium; start the heating function of the circulation system to raise the temperature of the circulation oil to 95°C. Put water under the sweating dish plate.

[0057] The wax oil product of the low-temperature F-T synthesis experimental device of China Petroleum & C...

Embodiment 2

[0075] This embodiment includes: (1) sweating and (2) emulsification.

[0076] (1) Sweating: Including (1) preparation, (2) cooling - high temperature constant temperature - cooling - low temperature constant temperature crystallization, (3) heating - constant temperature sweating, (4) refining four steps.

[0077] (1) Preparation

[0078] Connect the sealing system of the sweating dish with the pressurized buffer tank and the compressor; install the decompression buffer tank and connect the vacuum pump at the lower part of the sweating dish; connect the jacket of the sweating dish and the movable coil with the circulation system, and fix the coil in the On the sweating dish; use heat transfer oil as the heating medium; start the heating function of the circulation system to raise the temperature of the circulation oil to 95°C. Put water under the sweating dish plate.

[0079] The wax oil product (same as Example 1) of the low-temperature F-T synthesis experimental device of...

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Abstract

The invention discloses a method for preparing wax polish. According to the method, an F-T synthetic product is adopted as a raw material, and a target product is prepared through sweating and emulsification. On the basis of a common sweating process, a liquid component is carried out through a wax layer by virtue of air flow in the sweating process, then a solid component is compulsively separated from the liquid component, meanwhile preferably a sweating raw material forms stable micro bubbles in the wax layer under the action of a bubble stabilizer, a constant-temperature process is added in the crystallization process, then the liquid component can be rapidly discharged out, and thus a basic material without low-melting point components is produced; and the basic material is further emulsified with components such as silicon oil, natural wax and oil-soluble aids, and then a wax polish product is prepared. The method disclosed by the invention has the advantages of being low in production equipment investment, simple in production process, low in operation cost, safe and energy-saving, free of solvent pollution, good in wax polish product high temperature resistance, and the like.

Description

technical field [0001] The invention belongs to the technical field of production of daily-use chemical products, and in particular relates to a preparation method of glazing wax, especially a preparation method of glazing wax products suitable for various hard surfaces (floors, furniture, automobiles, etc.). Background technique [0002] Glazing products are mainly used to produce or restore the luster of various surfaces (floors, furniture, cars, etc.), and at the same time play a role in cleaning, anti-wear, anti-corrosion (wind and sun), waterproof, high temperature resistance, UV protection, anti-static, Anti-scratch and other effects. [0003] Polishing wax can be divided into solid, paste, liquid and other types according to different appearance. According to different dispersion media, it can be divided into solvent dispersion, emulsification dispersion and other types; in terms of composition, glazing wax includes volatile components, film-forming components and au...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09G1/12C10G73/36
CPCC09G1/12C10G73/36
Inventor 孙剑锋解利辉韩劲松郭慧兵张志银王士新
Owner CHINA PETROLEUM & CHEM CORP
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