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Method for calibrating partial cooling speed of electroslag ingot in process of producing high-speed steel through electroslag remelting

A local cooling and electroslag remelting technology, which is applied in the field of metallurgy, can solve problems such as the difficulty in achieving accurate control of the quality of electroslag ingots and the lack of quantitative characterization, and achieve the effects of detection effectiveness, fine carbide particles, and a safe and simple method

Active Publication Date: 2018-01-12
UNIV OF SCI & TECH LIAONING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

On the other hand, metallurgists control the solidification structure of electroslag ingots by adjusting process parameters such as slag system, slag amount, current, and voltage, but they have not realized the quantitative characterization of the process improvement effect, so it is difficult to achieve the electroslag ingot Accurate control of quality

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  • Method for calibrating partial cooling speed of electroslag ingot in process of producing high-speed steel through electroslag remelting
  • Method for calibrating partial cooling speed of electroslag ingot in process of producing high-speed steel through electroslag remelting
  • Method for calibrating partial cooling speed of electroslag ingot in process of producing high-speed steel through electroslag remelting

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Effect test

Embodiment 1

[0031]The principle of the cooling rate calibration method used in the production of electroslag ingots by electroslag remelting in the present invention is as follows (taking M42 high-speed steel as an example): first, cut out 20 samples of M42 (W2Mo9Cr4Co8) high-speed steel, and its specification is Ф7mm× 2.5mm, grinding and polishing to remove surface oxides; 20 groups of cooling rate experiments were designed respectively, and the experimental groups are shown in Table 1. Utilize ultra-high temperature laser confocal microscope to obtain the fully melted samples after the samples are solidified at different cooling rates; grind and polish the samples, and finally observe the microstructure image with the scanning electron microscope, and the carbonization of the fully melted samples obtained by electron microscope backscattering The object network distance is shown in Table 2, and the backscattered image of the fully melted sample is shown in Figure 3, where (a) 0.5°C / s, (b...

Embodiment 2

[0049] Electroslag remelting produces an M42 high-speed steel ingot with an ingot length of 1140 mm and a radius of 200 mm. The process parameters are shown in Table 3. A platinum-rhodium thermocouple was pre-embedded in the crystallizer (thermocouple position: 600mm in height, 15mm away from the crystallizer wall), and the measured cooling rate here was about 0.72°C / s. After the electroslag remelting is completed, the high-speed steel at the place where the thermocouple is embedded is made into a sample, and after grinding and polishing, it is observed with a scanning electron microscope, and its image is calculated and analyzed with an image analysis software (preferably Image-Pro-Plus). The average mesh distance of the carbides obtained is 49.09 μm; the distance between the carbide mesh of M42 high-speed steel observed by JSM6480LV scanning electron microscope (SEM), see Figure 4 ; The quantitative relationship between the average grid distance and the cooling rate brought...

Embodiment 3

[0053] Electroslag remelting produces an M42 high-speed steel with an ingot length of 1230 mm and a radius of 180 mm. The process parameters are shown in Table 4. A platinum-rhodium thermocouple was pre-embedded in the crystallizer (thermocouple position: 600mm in height, 55mm away from the crystallizer wall), and the cooling rate here was measured to be about 2.62°C / s. The high-speed steel at the place where the thermocouple is embedded is made into a sample, and after grinding and polishing, it is observed with a scanning electron microscope, and the image is calculated and analyzed with Image-Pro Plus image analysis software, and the average carbide mesh distance is 42.84μm; JSM6480LV Scanning electron microscope (SEM) observation of the measured M42 high-speed steel carbide network spacing, see Figure 5 ; The quantitative relationship between the average mesh distance and the cooling rate of the carbides brought into M42 high-speed steel, where the cooling rate is about 2...

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Abstract

The invention belongs to the technical field of metallurgy, particularly relates to a method for calibrating partial cooling speed of an electroslag ingot in a process of producing high-speed steel through electroslag remelting and specifically relates to a method for accurately controlling the quality of high-speed steel carbide by calibrating the partial cooling speed of the electroslag ingot ofthe high-speed steel. The method is used for studying the quantitative relationship between the cooling speed of the electroslag ingot in the process of producing the high-speed steel through electroslag remelting by measuring the corresponding relationship between the characteristics of the high-speed steel carbide and the partial cooling speed, and a quantitative relationship curve and a relational expression of the cooling speed of the electroslag ingot and the characteristics of the carbide are obtained by statistics and calculation of the characteristics of the carbide at different cooling speeds; the cooling speed of partial solidification is effectively determined according to an off-contact distance of the carbide of the electroslag ingot; therefore, in the actual production of the high-speed steel, the cooling speed of the partial solidification can be changed directly by adjusting the technological parameters of the electroslag remelting, so that the electroslag ingot meeting the quality requirements of the required carbide is obtained.

Description

technical field [0001] The invention belongs to the technical field of metallurgy, and in particular relates to a method for calibrating the local cooling speed of electroslag ingots in the process of producing high-speed steel by electroslag remelting, specifically, by calibrating the local cooling speed of high-speed steel electroslag ingots, thereby precisely controlling the carbonization of high-speed steel method of material quality. Background technique [0002] The electroslag remelting method is the main method to prepare high-quality high-speed steel. Its advantages include less non-metallic inclusions, high metal purity, uniform crystal structure in the center of the ingot, compact structure, and good surface quality of the ingot. [0003] The carbon saturation in high-speed steel is high, and the number of eutectic carbides is large. The carbides form a continuous network to separate the matrix, making the plasticity of the steel poor, and the primary carbides in ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N23/22C22B9/18
Inventor 李万明耿一峰孙梦茹臧喜民邓鑫姜周华
Owner UNIV OF SCI & TECH LIAONING