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Strontium phosphate-based nano-assembling spherical anticorrosive pigment

A nano-assembly and anti-corrosion pigment technology, applied in the field of material chemistry, can solve the problems that there are no research reports on the preparation of strontium phosphate-based nano-assembly spherical anti-corrosion pigments, and achieve the effects of stable structure, small particle size, and fixed chemical composition

Active Publication Date: 2018-02-02
EAST CHINA UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Through the investigation of the types and preparation technologies of existing anti-corrosion pigments, it is found that there is no research report on the preparation of strontium phosphate-based nano-assembled spherical anti-corrosion pigments

Method used

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  • Strontium phosphate-based nano-assembling spherical anticorrosive pigment

Examples

Experimental program
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Effect test

Embodiment 1

[0020] Prepare strontium nitrate and 0.8 mol / L sodium phosphate solutions with a concentration of 1.2 mol / L respectively, measure 25 mL of the above two solutions and place them in two beakers, add 0.2 g of benzene to the strontium nitrate and sodium phosphate solutions respectively Triazole and 0.05g polyethylene glycol, stirred until fully dissolved. Place the strontium nitrate solution and the sodium phosphate solution on both sides of the egg membrane respectively. After reacting for 12 hours, take the precipitate, wash it with deionized water three times, put it in an oven, and dry it at 60°C for 12 hours to obtain the strontium phosphate base. Nano-assembled spherical anti-corrosion pigments. The overall diameter of the obtained strontium phosphate-based nano-assembled spherical anticorrosion pigment is about 2.5 μm, and the thickness of the nanoribbon assembled into the nano-assembled sphere is about 30 nm. The anti-corrosion pigment is added to the paint to make a pai...

Embodiment 2

[0022] Prepare strontium nitrate and 0.008mol / L sodium phosphate solutions with a concentration of 0.012 mol / L respectively, measure 25 mL of the above two solutions and place them in two beakers, add 0.01 g of benzene to the strontium nitrate and sodium phosphate solutions respectively Triazole and 0.02g cetyltrimethylammonium bromide, stirred until fully dissolved. Place the strontium nitrate solution and the sodium phosphate solution on both sides of the egg membrane respectively. After reacting for 12 hours, take the precipitate, wash it with deionized water three times, put it in an oven, and dry it at 60°C for 12 hours to obtain the strontium phosphate base. Nano-assembled spherical anti-corrosion pigments. The overall diameter of the obtained strontium phosphate-based nano-assembled spherical anticorrosion pigment is about 3 μm, and the thickness of the nanobelt assembled into the nano-assembled sphere is about 22 nm. The anti-corrosion pigment is added to the paint to...

Embodiment 3

[0024] Prepare strontium nitrate and 0.0008mol / L sodium phosphate solutions with a concentration of 0.0012 mol / L respectively, measure 25 mL of the above two solutions and place them in two beakers, add 0.001 g of benzene to the strontium nitrate and sodium phosphate solutions respectively And triazole and 0.0125g polyacrylamide, stir until it is fully dissolved. Place the strontium nitrate solution and the sodium phosphate solution on both sides of the egg membrane, react for 12 hours, take the precipitate, wash it with deionized water 3 times, put it in an oven, and dry it at 95°C for 1 hour to obtain the strontium phosphate base Nano-assembled spherical anti-corrosion pigments. The overall diameter of the obtained strontium phosphate-based nano-assembled spherical anticorrosion pigment is about 2.5 μm, and the thickness of the nanoribbon assembled into the nano-assembled sphere is about 20 nm. The anti-corrosion pigment is added to the paint to make a paint film. The resul...

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Abstract

The invention belongs to the technical field of material chemistry and particularly relates to a preparation method of strontium phosphate-based nano-assembling spherical anticorrosive pigment. The strontium phosphate-based nano-assembling spherical anticorrosive pigment is of an ordered structure assembled by nanobelts, and the surface of the pigment can be firmly composited with benzotriazole and a surfactant. The strontium phosphate-based nano-assembling spherical anticorrosive pigment 2-3 micrometers in overall diameter and prepared from the nanobelts 20-30 nm thick has the advantages of good dispersity, excellent compatibility and excellent corrosion resistant performance.

Description

technical field [0001] The invention belongs to the field of material chemistry, and in particular relates to a strontium phosphate-based nano-assembled spherical anti-corrosion pigment and a preparation method thereof. Background technique [0002] The biggest advantage of phosphate series anti-corrosion pigments is that they are environmentally friendly and belong to non-toxic anti-corrosion pigments. Phosphate has good compatibility in various coating systems, and under high temperature conditions, phosphate can produce pyrophosphate that is more stable and less volatile. In silicone high-temperature coating products, phosphate is also a better anti-corrosion agent. rust paint. At present, the main types of relatively mature phosphate series products in the market are orthophosphate, polyphosphate, pyrophosphate and metaaluminate. [0003] As an important phosphate, strontium phosphate is often used in the field of luminescent materials and cement modified fillers. As ...

Claims

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Application Information

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IPC IPC(8): C09D5/08
CPCC09D5/082C09D5/084C09D5/086
Inventor 刘金库刘修芮王可心周丹孙一硕张敏薛亚楠袁晓宇苗敏
Owner EAST CHINA UNIV OF SCI & TECH
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