Compound, colorant composition containing same and resin composition containing same
A technology for compounds and compositions, applied in the fields of compounds, colorant compositions containing them and resin compositions containing them, can solve problems such as difficult adjustment, achieve excellent solubility, improve heat resistance and chemical resistance, The effect of excellent heat resistance and chemical resistance
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manufacture example 1
[0202] Production Example 1. Manufacture of Compound 1
[0203]
[0204] 11.59 (15.23 mmol) of B-1 and 2.5 g (15.23 mmol) of A-1 was added to 700 g of pyridine, stirred at room temperature for 24 hours. The reaction was added to Di water and stirred for 1 hour. The precipitate was filtered and washed with water under reduced pressure, and dried at 80 ° C for 12 hours. Thereafter, the dried precipitate was obtained by column chromatography.
[0205] Ionization mode =: APCI +: m / z = 928 [M + H] +, Exact Mass: 927
manufacture example 2
[0206] Production Example 2. Made of Compound 2
[0207]
[0208] In the above-described example 1, C-1 is used instead of B-1, and the compound 2 is obtained in the same manner.
[0209]Ionization mode =: APCI +: m / z = 984 [m + h] +, exact mass: 983
manufacture example 3
[0210] Production Example 3. Manufacture of Compound 3
[0211]
[0212] In the above-described example 1, the compound 3 is obtained in the same manner as the B-1 is used, and the compound 3 is obtained in the same manner.
[0213] Ionization mode =: APCI +: m / z = 1040 [M + H] +, Exact Mass: 1039
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