Novel compound, core-shell dye, photosensitive resin composition and color filter
A photosensitive resin and compound technology, applied in the field of color filters, can solve problems such as poor durability, light resistance, heat resistance, and brightness degradation
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Synthetic example 1
[0280] (Synthesis Example 1: Synthesis of Intermediate A)
[0281]
[0282] Added aniline (10mol), 4-bromotoluene (10mol), Pd 2 (dba) 3 (0.1 mol) and Xphos (0.1 mol), and the mixture was heated and stirred at 100°C for 24 hours. To this solution was added ethyl acetate, and the obtained mixture was washed twice with water to extract an organic layer. The extracted organic layer was distilled under reduced pressure and purified by column chromatography to obtain Intermediate A.
Synthetic example 2
[0283] (Synthesis Example 2: Synthesis of Intermediate B-1)
[0284]
[0285] Added 2,4-dimethyldiphenylamine (10mol), 1,2-epoxyhexane (12mol) and sodium hydride (12mol) to N,N-dimethylformamide, and at 90°C The mixture was heated and stirred for 24 hours. To this solution was added ethyl acetate, and the obtained mixture was washed twice with water to extract an organic layer. The extracted organic layer was distilled under reduced pressure and separated by column chromatography to obtain Intermediate B-1.
Synthetic example 3
[0286] (Synthesis Example 3: Synthesis of Intermediate B-2)
[0287]
[0288] Intermediate B-2 was synthesized in the same manner as in Synthesis Example 2 except that 1,2-epoxybutylene was used instead of 1,2-epoxyhexane.
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