Acrylic fiber conductive filament and method for preparing same by aid of complexation and doping processes
A technology of conductive filament and acrylic fiber, which is applied in the field of preparation of acrylic conductive filament and its complex doping method, can solve the problems of large pollution, conductive stability, less application, etc. The effect of comfort, good electrical resistance
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Embodiment 1
[0046] 1. The untwisted acrylic filaments are stretched and twisted on the puller, and the shrinkage of the treated filaments in boiling water is ≤1.5%, and the twist is 96 twists / m.
[0047] 2. The bobbin after elastic twisting is wound on the loose bobbin, and the density is controlled at 0.25Kg / dm 3 .
[0048] 3. Place the loose yarn bobbin in a closed container for deoiling treatment in the form of two-way pressure washing. After deoiling treatment, wash it with water three times to centrifugally dehydrate the yarn bobbin.
[0049] 4. Place the loose yarn bobbin in a closed container to micro-etch and roughen the surface of the fiber in the form of two-way pressure washing. After the treatment, wash the bobbin three times with water to centrifugally dehydrate the bobbin.
[0050] 5. Place the loose yarn bobbin in a closed container to activate the fiber under acidic conditions in the form of two-way pressure impregnation.
[0051] 6. Place the loose yarn bobbin in a clos...
Embodiment 2
[0055] The difference from Example 1 is:
[0056] 6. Place the loose yarn bobbin in a closed container to carry out the copper coating on the surface of the fiber in the form of two-way pressure impregnation. 2+ Dipping. The yarn ratio of each component of the impregnation solution is: 16% copper sulfate, 0.1% triethanolamine, and an appropriate amount of sulfuric acid. 2+ Uniform adsorption, diffusion and penetration from the fiber surface to the inside.
[0057] 7. Place the impregnated yarn bobbin in a closed container in the form of two-way pressure impregnation at a temperature of 100°C and a pressure of 0.20MPa to achieve Cu adsorption on the fiber surface. 9 S 5 The complexation generation, the yarn ratio of each component of the complexation reaction solution is: copper sulfate 16%, sodium thiosulfate 18%, silver nitrate 0.08%, polyethylene glycol 0.1%, edetate disodium 0.1%, the reaction produces Cu 9 S 5 , doped with 0.5%-1% silver ions, and finally form a dark...
Embodiment 3
[0059] The difference from Example 1 is:
[0060] 6. Place the loose yarn bobbin in a closed container to carry out the copper coating on the surface of the fiber in the form of two-way pressure impregnation. 2+ Dipping. The yarn ratio of each component of the impregnation solution is: 18% copper sulfate, 0.1% triethanolamine, and an appropriate amount of sulfuric acid. 2+ Uniform adsorption, diffusion and penetration from the fiber surface to the inside.
[0061] 7. Place the impregnated yarn bobbin in a closed container in the form of two-way pressure impregnation at a temperature of 100°C and a pressure of 0.20MPa to achieve Cu adsorption on the fiber surface. 9 S 5 The complexation generation, the yarn ratio of each component of the complexation reaction solution is: copper sulfate 16%, sodium thiosulfate 18%, silver nitrate 0.06%, polyethylene glycol 0.1%, edetate disodium 0.1%, the reaction produces Cu 9 S 5 , doped with 0.5%-1% silver ions, and finally form a dark...
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