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A kind of environment-friendly interior wall coating and preparation method thereof

An interior wall coating and environmental protection technology, applied in the direction of fireproof coating, antifouling/underwater coating, coating, etc., can solve the problems of poor bonding ability, difficult construction, poor fire protection level, etc., and achieve good absorption and decomposition of formaldehyde Ability, simple and easy preparation method, fireproof performance and strong bonding ability

Inactive Publication Date: 2020-05-15
南通涂冠环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The invention object of the present invention is to provide a kind of environment-friendly interior wall coating and preparation method thereof, and this preparation method is simple and easy, and equipment requirement is not high, and component is easy to obtain, aftertreatment is convenient, and price is low, is suitable for large-scale production; Prepared The environmentally friendly interior wall coating overcomes the defects of the existing traditional interior wall coatings such as high cost, poor fire rating, difficult construction, poor bonding ability, easy to fall off, and easy release of formaldehyde, causing environmental pollution that threatens people's health.

Method used

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  • A kind of environment-friendly interior wall coating and preparation method thereof

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Embodiment 1

[0038]An environment-friendly interior wall paint, comprising the following components by weight: 35 parts of fluorine-containing triazine film-forming polymer, 10 parts of phosphonic acid-modified nano-titanium dioxide, 20 parts of rutile titanium dioxide, 2 parts of tributyl phosphate, 3 parts of propylene glycol, 20 parts of water.

[0039] The preparation method of described fluorine-containing triazine film-forming polymer comprises the steps:

[0040] 1) Add 10g of glycidyl methacrylate, 4,6-bis(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-amine (CAS: 301211-00-7 ) 20g into 100g of isopropanol, and 0.1g of the polymerization inhibitor chlorobenzoquinone was added therein, stirred and reacted at 80°C for 6 hours, then the solvent was removed by rotary evaporation, then washed 4 times with ether, and the ether was removed by rotary evaporation again ;

[0041] 2) Add 10g of glycidyl methacrylate and 20g of 2,4-dioxohexahydro-1,3,5-triazine (CAS: 27032-78-6) into 100g of tetrah...

Embodiment 2

[0049] An environment-friendly interior wall paint, comprising the following components in parts by weight: 38 parts of fluorine-containing triazine film-forming polymer, 12 parts of phosphonic acid-modified nano-titanium dioxide, 23 parts of lithopone, and 3 parts of defoamer Deqian 3100 , 4 parts of methyl ether, 23 parts of water.

[0050] The preparation method of described fluorine-containing triazine film-forming polymer comprises the steps:

[0051] 1) Add 10g of glycidyl methacrylate, 4,6-bis(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-amine (CAS: 301211-00-7 ) 25g into 120g of dichloromethane, and 0.15g of chloranil, a polymerization inhibitor, was added thereto, stirred and reacted at 83°C for 6.5 hours, then the solvent was removed by rotary evaporation, and washed 5 times with ether, and the ether was removed by rotary evaporation again ;

[0052] 2) Add 10g of glycidyl methacrylate and 25g of 2,4-dioxohexahydro-1,3,5-triazine (CAS: 27032-78-6) into 125g of tetrahydro...

Embodiment 3

[0060] An environment-friendly interior wall paint, comprising the following components by weight: 40 parts of fluorine-containing triazine film-forming polymer, 14 parts of phosphonic acid modified nano-titanium dioxide, 27 parts of heavy calcium carbonate, 4 parts of defoamer BYK0888, propylene glycol 5 parts of butyl ether, 26 parts of water.

[0061] The preparation method of described fluorine-containing triazine film-forming polymer comprises the steps:

[0062] 1) Add 10g of glycidyl methacrylate, 4,6-bis(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-amine (CAS: 301211-00-7 ) 26 g into 135 g of acetone, and 0.22 g of the polymerization inhibitor chlorobenzoquinone was added therein, stirred and reacted at 86° C. for 7 hours, then the solvent was removed by rotary evaporation, and then washed 6 times with ether, and the ether was removed by rotary evaporation again;

[0063] 2) Add 10g of glycidyl methacrylate and 25g of 2,4-dioxohexahydro-1,3,5-triazine (CAS: 27032-78-6) into...

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Abstract

The invention discloses environment-friendly inner wall paint, which is prepared from the following ingredients in parts by weight: 35 to 45 parts of fluorine-containing triazine type film forming polymers, 10 to 15 parts of phosphoric acid modified nanometer titanium dioxide, 20 to 30 parts of pigment filling materials, 2 to 5 parts of anti-foaming agents, 3 to 7 parts of coalescing agents and 20to 30 parts of water. The preparation method of the environment-friendly inner wall paint comprises the following steps that the fluorine-containing triazine type film forming polymers, the phosphoric acid modified nanometer titanium dioxide, the pigment filling materials, the anti-foaming agents, the dispersing agents and the coalescing agents are proportionally put into a high-speed mixing machine to be mixed for 20 to 30min, and are then charged into a ball milling tank; after the ball milling treatment is performed for 5 to 8h, mixed powder is obtained; then, water is added into the mixedpowder; at the rotating speed being 1200 to 1500 turns per minute, dispersion is performed for 10 to 15 minutes; next, curing is performed for 2 to 5 days; sampling for inspection is performed; afterthe products are qualified, sieving and packaging are performed. The environment-friendly inner wall paint disclosed by the invention has the advantages that the price is cheap; the formaldehyde absorption and decomposition effects are obvious; the efficiency is high; the secondary pollution cannot be caused; the visible light response speed is high; the fireproof performance and the bonding capability are high; the weathering performance is good.

Description

technical field [0001] The invention relates to the technical field of building decoration materials, in particular to an environmentally friendly interior wall paint and a preparation method thereof. Background technique [0002] In recent years, with the improvement of people's living standards, various decorative and decorative coatings emerge in an endless stream. While these decorative and decorative coatings bring people a sense of comfort, they also bring about increasingly serious environmental problems. The body takes a fatal toll. As one of the decorative paints, interior wall paint is closely related to people's life and work because it is directly painted on the inner surface of buildings or structures. More attention should be paid to the toxicity and tasteless characteristics. [0003] The important substance that interior wall paint pollutes the indoor air environment is formaldehyde. It is mainly released through the degradation of wood adhesives and plasti...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D133/16C09D5/18C09D5/14C09D7/62C09D7/20C08F220/36C08F220/14
CPCC08F220/36C08K9/04C08K2003/2241C08K2201/011C09D5/14C09D5/18C09D133/16C08F220/14
Inventor 董廷显秦岩
Owner 南通涂冠环保科技有限公司
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