Humic acid activation method and device

An activation method and humic acid technology, which are applied in fertilization devices, ammonium orthophosphate fertilizers, alkaline orthophosphate fertilizers, etc., can solve the problem of low activation performance and output rate of products, long reaction time and production cycle, and poor activation effect. and other problems, to achieve good activation effect, high output rate, and the effect of promoting chlorophyll synthesis

Active Publication Date: 2018-05-18
SHANDONG AGRI UNIV FERTILIZER TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, conventional humic acid activation methods include oxidation activation, alkalization activation, etc., all of which undergo a series of process equipment such as activation extraction, solid-liquid separation, evaporation and drying under liquid phase conditions, which have cumbersome processes, high energy consumption, and pollution. Large and other disadvantages, and the conventional activation method is mostly carried out at normal temperature and pressure, the reaction time and production cycle are long, the activation effect is poor, the activation performance and output rate of the product are low

Method used

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  • Humic acid activation method and device
  • Humic acid activation method and device
  • Humic acid activation method and device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0077] The embodiment of the present invention provides a humic acid activation device, which includes two reaction kettles 1, a steam curing car 2 and a transport traction device for moving the steam curing car 2 in the reactor 1, the transportation The traction device is connected to the steam-curing vehicle 2, the steam-curing vehicle 2 is located in the reaction kettle 1, and the steam-curing vehicle 2 is provided with a material cage for placing raw materials.

[0078]The two reaction kettles 1 are communicated with each other through a sub-cylinder 3, and a control valve 5 is respectively arranged on the communication pipeline between the two described reaction kettles 1 and the sub-cylinder 3, and the sub-cylinder 3 is communicated through a steam pipeline 4. Steam supply device. Pressure safety valves 6, steam traps, thermometers and pressure gauges are installed on the two reactors 1 to adjust and control the reaction temperature and reaction pressure of the materials...

Embodiment 2

[0085] Based on the above-mentioned humic acid activation device, the humic acid activation method provided in this embodiment is:

[0086] Mix humic acid raw materials, oxidants and activators at a weight ratio of 1:0.05:0.05 to obtain a mixture. Stir the mixture and water evenly at a weight ratio of 1:0.2 and place it in a room with a temperature of 200°C and a pressure of 1.5MPa. Steaming and reacting under saturated water vapor for 2 hours; then cooling, drying and crushing to obtain active humic acid.

[0087] The described humic acid activation method is applied to the above-mentioned device, and the specific implementation steps are:

[0088] (1) Mix the humic acid raw material, oxidizing agent and activator at a weight ratio of 1:0.05:0.05 to obtain a mixture, mix the mixture and water evenly at a weight ratio of 1:0.2, and then put them into each material cage, Code is put on the steam maintenance car 2.

[0089] (2) Transport the steaming vehicles 2 in step (1) to ...

Embodiment 3

[0096] The humic acid activation device provided in this embodiment is the same as the above-mentioned embodiment 2, the difference is that the humic acid activation method in this embodiment is:

[0097] Mix the humic acid raw material, oxidizing agent and alkalizing agent in a weight ratio of 1:0.2:0.2 to obtain a mixture, then stir the mixture and water evenly in a weight ratio of 1:0.5 and place it at a temperature of 170°C and a pressure of Under 0.8MPa saturated water vapor, it was steamed and reacted for 5 hours; then cooled, dried and pulverized to obtain active humic acid. The specific implementation steps of applying the humic acid activation method to the humic acid activation device are the same as the above-mentioned embodiments.

[0098] In the products obtained in this example, the activated humic acid content is 80% to 98%, and the activation degree is greater than or equal to 99%.

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Abstract

The invention provides a humic acid activation method and device. The method comprises steps as follows: a humic acid raw material is mixed with an activating agent, and after water is added and stirring is performed, a mixture is subjected to steam curing in high-temperature and high-pressure saturated steam; correspondingly, the humic acid activation device comprises two reaction kettles which are communicated through a steam distribution header, the steam distribution header is communicated with a steam supply device, steam curing cars are arranged in the reaction kettles, after the humic acid raw material is mixed with the activating agent, water is added and stirring is performed, the mixture is placed on the steam curing cars, and the steam curing cars are put in the corresponding reaction kettles for steam curing reaction. The humic acid is activated under stream pressure, so that the reaction time is shortened, the technology is simple, the energy consumption is low, and the activation effect is good; the two reaction kettles are arranged and can be used for performing the steam curing reaction alternately, continuous production of active humic acid is realized, the production cycle is shortened, and the efficiency is improved.

Description

technical field [0001] The invention relates to the technical field of humic acid activation, in particular to a humic acid activation method and device. Background technique [0002] At present, conventional humic acid activation methods include oxidation activation, alkalization activation, etc., all of which undergo a series of process equipment such as activation extraction, solid-liquid separation, evaporation and drying under liquid phase conditions, which have cumbersome processes, high energy consumption, and pollution. Large and other disadvantages, and the conventional activation method is mostly carried out at normal temperature and pressure, the reaction time and production cycle are long, the activation effect is poor, and the activation performance and output rate of the product are low. Therefore, it is urgent to find a humic acid activation method and device that is more conducive to production. Contents of the invention [0003] Aiming at the deficiencies...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08H7/00C05G3/04C05G1/00C05G3/80
CPCC05B7/00C08H6/00C05G3/80C05C9/00C05D1/02C05D9/00C05F11/02C05C11/00C05C3/00C05D9/02
Inventor 丁方军吴钦泉路艳艳陈士更朱福军陈光峰张宏
Owner SHANDONG AGRI UNIV FERTILIZER TECH CO LTD
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