Catalytic cracking oil slurry solid-removing agent and preparation method thereof
A technology for catalytic cracking oil slurry and catalyst, which is applied in the petroleum industry, refining hydrocarbon oil, etc., can solve the problems of the adverse effect of the deep utilization of oil slurry, affecting the quality of oil slurry, affecting the removal efficiency, etc., to promote coalescence, fast speed , the effect of less dosage
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Embodiment 1
[0027] Embodiment 1: the preparation of oil slurry desolidifying agent A
[0028] (1) Preparation of solid release agent main agent:
[0029] a. In a 250mL four-neck flask equipped with a thermometer, water separator and reflux condenser, add 20g of polyoxyethylene polyoxypropylene block copolymer (molecular weight about 2000), 2g of maleic anhydride (polyoxyethylene polyoxypropylene The molar ratio of block copolymer to maleic anhydride is 1:2), 0.3g p-toluenesulfonic acid (p-toluenesulfonic acid accounts for 1.5% of the total mass of the reactant) and 150mL toluene, and the temperature is raised to 140°C for reaction. The water output in the water separator judges the progress of the reaction, the total reaction time is 6 hours, and polyoxyethylene polyoxypropylene ether maleate is obtained.
[0030] b. In a 250mL four-necked flask equipped with a thermometer, a water separator and a reflux condenser, add 20g of polytetrahydrofuran (molecular weight is about 2000), 2g of ma...
Embodiment 2
[0034] Embodiment 2: the preparation of oil slurry desolidifying agent B
[0035] (1) Preparation of solid release agent main agent:
[0036] a. In a 250mL four-neck flask equipped with a thermometer, water separator and reflux condenser, add 20g of polyoxyethylene polyoxypropylene block copolymer (molecular weight about 2000), 1g of maleic anhydride (polyoxyethylene polyoxypropylene The molar ratio of block copolymer to maleic anhydride is 1:1), 0.2g p-toluenesulfonic acid (p-toluenesulfonic acid accounts for 1% of the total mass of the reactant) and 150mL toluene, and the temperature is raised to 130°C for reaction. The water output in the water separator judges the progress of the reaction, the total reaction time is 4 hours, and polyoxyethylene polyoxypropylene ether maleate is obtained.
[0037] b. In a 250mL four-necked flask equipped with a thermometer, a water separator and a reflux condenser, add 20g of polytetrahydrofuran (molecular weight is about 2000), 1g of male...
Embodiment 3
[0041] Embodiment 3: the preparation of oil slurry desolidification agent C
[0042] (1) Preparation of solid release agent main agent:
[0043] a. In a 250mL four-necked flask equipped with a thermometer, water separator and reflux condenser, add 20g of polyoxyethylene polyoxypropylene block copolymer (molecular weight about 2000), 3g of maleic anhydride (polyoxyethylene polyoxypropylene The molar ratio of block copolymer to maleic anhydride is 1:3), 0.5g p-toluenesulfonic acid (p-toluenesulfonic acid accounts for 2% of the total mass of the reactant) and 150mL toluene, and the temperature is raised to 160°C for reaction. The water output in the water separator judges the progress of the reaction, the total reaction time is 8 hours, and polyoxyethylene polyoxypropylene ether maleate is obtained.
[0044] b. In a 250mL four-necked flask equipped with a thermometer, a water separator and a reflux condenser, add 20g of polytetrahydrofuran (molecular weight is about 2000), 3g of...
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