Method for preparing composite polypropylene shell of automobile igniter
A technology for compounding polypropylene and automobile points, which is applied in the field of preparing compound polypropylene automobile igniter shells, can solve the problems of high temperature sensitivity and limited application, and achieves low high temperature sensitivity, improved Vicat softening point, and thermal stability. effect of effect
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Embodiment 1
[0018] A preparation method for a composite polypropylene automobile igniter shell, comprising the steps of:
[0019] S1. Mix 50g polypropylene, 30g chlorosulfonated polyethylene, 2g monoalkoxy unsaturated fatty acid titanate, and 4g epoxy resin, heat up to 70°C and stir for 30min, add 6g styrene-butadiene rubber, 12g zinc oxide, 6g Diatomite, 8g of hard clay, 5g of medical stone powder, 10g of expanded perlite, 15g of nano-titanium dioxide, heated up to 95°C and continued to stir for 5min, cooled to obtain premix a;
[0020] S2. Add 2g of 1,1-bis-(tert-butylperoxy)cyclohexane, 2.5g of triethylenetetramine, 2g of light stabilizer, and 5g of antioxidant to 120g of the premixed material, raise the temperature to 110°C and continue stirring for 8min. Get premix b;
[0021] S3. Extrude and granulate the premix b through a twin-screw extruder. The barrel temperature of the extruder is 170°C in the first zone, 195°C in the second zone, 205°C in the third zone, and 200°C in the four...
Embodiment 2
[0023] A preparation method for a composite polypropylene automobile igniter shell, comprising the steps of:
[0024] S1. Mix 70g polypropylene, 20g chlorosulfonated polyethylene, 4g monoalkoxy unsaturated fatty acid titanate, and 2g epoxy resin, heat up to 80°C and stir for 20min, add 14g styrene-butadiene rubber, 6g zinc oxide, 12g Diatomite, 4g of hard clay, 9g of medical stone powder, 6g of expanded perlite, 25g of nano-titanium dioxide, heated up to 85°C and continued to stir for 12min, cooled to obtain premix a;
[0025] S2. Add 4g of 1,1-bis-(tert-butylperoxy)cyclohexane, 1.5g of triethylenetetramine, 4g of light stabilizer, and 3g of antioxidant to 100g of the premix, heat up to 118°C and continue stirring for 2min. Get premix b;
[0026] S3. Extrude and granulate the premix b through a twin-screw extruder. The temperature of the first zone of the extruder barrel is 178°C, the temperature of the second zone is 185°C, the temperature of the third zone is 215°C, and the...
Embodiment 3
[0028] A preparation method for a composite polypropylene automobile igniter shell, comprising the steps of:
[0029] S1. Mix 55g polypropylene, 28g chlorosulfonated polyethylene, 2.5g monoalkoxy unsaturated fatty acid titanate, and 3.5g epoxy resin, heat up to 73°C and stir for 28min, add 8g styrene-butadiene rubber, 10g zinc oxide , 8g diatomite, 7g hard clay, 6g medical stone powder, 9g expanded perlite, 18g nano-titanium dioxide, heat up to 92°C and continue stirring for 8min, cool to obtain premix a;
[0030] S2. Add 2.5g of 1,1-bis-(tert-butylperoxy)cyclohexane, 2.2g of triethylenetetramine, 2.5g of light stabilizer, and 4.5g of antioxidant to 115g of the premix, and heat up to 112°C to continue Stir for 6min to obtain premix b;
[0031] S3. Extrude and granulate the premix b through a twin-screw extruder. The barrel temperature of the extruder is 172°C in the first zone, 192°C in the second zone, 208°C in the third zone, and 198°C in the fourth zone. , the mold temper...
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