Chiral poly-schiff base cobalt salt composite wave-absorbing material
A technology of composite absorbing material and Schiff base cobalt salt, which is applied in the field of absorbing materials to achieve the effects of small specific gravity, wide absorbing frequency and preventing volatilization
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0025] (1) Dissolve 0.04 mol of ferrocene formaldehyde in 80 ml of methanol, and raise the temperature to 45° C. under reflux to obtain a ferrocene formaldehyde methanol solution.
[0026] (2) Dissolve 0.02mol of chiral (R,R)-1,2-diphenylethylenediamine in 40ml of methanol, and then dissolve chiral (R,R)-1,2-diphenylethylenediamine The methanol solution was slowly dropped into the ferrocene formaldehyde methanol solution. After the drop was completed within 25 minutes, the solution was stirred and refluxed under nitrogen protection at 45°C for 6 hours to obtain solution A.
[0027] (3) The solution A was filtered, and the resulting filter cake was vacuum-dried at 35° C. for 24 hours to obtain a chiral ferrocenyl bis-Schiff base.
[0028] (4) Dissolve 0.1 mol of aluminum trichloride in 60 ml of chloroform, and drop into 12 ml of chloroform solution containing 0.01 mol of sebacoyl chloride to obtain solution B.
[0029] (5) Dissolve 0.01mol of chiral ferrocenyl bis-Schiff base ...
Embodiment 2
[0038] (1) Dissolve 0.06 mol of ferrocene formaldehyde in 60 ml of methanol, and raise the temperature to 45° C. under reflux to obtain a methanol solution of ferrocene formaldehyde.
[0039] (2) Dissolve 0.03mol of chiral (R)-(+)-2,2-diamino-1,1-binaphthyl in 30ml of methanol, and then dissolve chiral (R)-(+)-2,2 -Diamino-1,1-binaphthyl methanol solution was slowly dropped into the ferrocene formaldehyde methanol solution. After the drop was completed within 25 minutes, the mixture was stirred and refluxed under nitrogen protection at 45°C for 6 hours to obtain solution A.
[0040] (3) The solution A was filtered, and the resulting filter cake was vacuum-dried at 35° C. for 24 hours to obtain a chiral ferrocenyl bis-Schiff base.
[0041] (4) Dissolve 0.2 mol of aluminum trichloride in 120 ml of chloroform, and drop into 20 ml of chloroform solution containing 0.02 mol of sebacoyl chloride to obtain solution B.
[0042] (5) Dissolve 0.02mol of chiral ferrocenyl bis-Schiff bas...
PUM
Property | Measurement | Unit |
---|---|---|
Thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com