High-density oil-based drilling fluid plugging liquid and preparation method and application thereof
An oil-based drilling fluid and high-density technology, which is applied in the field of oil well plugging, can solve the problems of unfavorable oil layer acidification reform, easy subsidence or floating, and high overall concentration of plugging fluid, so as to improve the ability and hardness of supporting pores and fractures Excellent flexibility and high compressive strength
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Embodiment 1
[0050] 1. Raw material preparation
[0051] (1) Drilling mud
[0052] Select the drilling mud used in the oil field.
[0053] (2) Aluminum alloy particles GYD
[0054] The density of aluminum alloy particles GYD is 2.3-2.6g / cm 3 , the fineness is 6.7-0.17mm.
[0055] (3) Non-penetration treatment agent BYD
[0056] (4) High acid soluble calcium granule KGD
[0057] High acid soluble calcium granules KGD, density 2.6-2.7g / cm 3 , the particle size is 0.3mm ~ 3.00mm.
[0058] 2. Preparation of high-density oil-based drilling fluid plugging fluid
[0059] Prepare high-density oil-based drilling fluid plugging fluid according to the following weight percentages:
[0060] Aluminum alloy particles GYD (6.7-4mm) 1%, aluminum alloy particles GYD (4.0-1.4) 1%, aluminum alloy particles GYD (1.4-0.28mm) 1%; aluminum alloy particles GYD (0.28-0.17mm) 1%.
[0061] Non-permeable treatment agent BYD 5%; high acid soluble calcium particles KGD (0.3mm ~ 0.45mm) 2%, high acid soluble ca...
Embodiment 2
[0064] 1. Raw material preparation
[0065] (1) Drilling mud
[0066] Select the drilling mud used in the oil field.
[0067] (2) Aluminum alloy particles GYD
[0068] The density of aluminum alloy particles GYD is 2.3-2.6g / cm 3 , the fineness is 6.7-0.17mm.
[0069] (3) Non-penetration treatment agent BYD
[0070] (4) High acid soluble calcium granule KGD
[0071] High acid soluble calcium granules KGD, density 2.6-2.7g / cm 3 , the particle size is 0.3mm ~ 3.00mm.
[0072] (5) Flexible polymer materials
[0073] (i) Preparation of (meth)acrylate rubber
[0074] (a) 60g of 2-ethylhexyl acrylate and 12g of ethylene difluoride are mixed uniformly;
[0075] (b) 1g benzoyl peroxide is added in 100g cyclohexanone, and stir;
[0076] (c) adding the xylene solution in step (ii) to the monomer mixture in step (i), initiating a polymerization reaction at 60-90° C. to obtain (meth)acrylate rubber.
[0077] (ii) Preparation of flexible polymer materials
[0078] (a) Add 45g of...
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