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Polarized light microscopy-X-ray diffraction method for qualitative detection of asbestos in electronic products

An electronic product and polarizing microscopy technology, which is applied in the direction of material analysis using wave/particle radiation, measuring devices, and material analysis through optical means, can solve the complex structure of asbestos components, difficulty in achieving results, and low universality. and other issues to achieve the effect of avoiding trade risks, avoiding asbestos hazards, and good reproducibility

Inactive Publication Date: 2018-08-24
CHINESE ACAD OF INSPECTION & QUARANTINE
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Problems solved by technology

For the detection of trace asbestos in electronic products, the existing technology is not perfect
X-ray diffraction is based on the proportional relationship between the content of a certain mineral and the intensity of its diffraction peak to judge whether a sample contains a certain asbestos mineral and determine its content. Since serpentine and hornblende minerals themselves have a fibrous structure or non- There are two kinds of fiber structure, serpentine and hornblende with fiber structure are called asbestos, so using X-ray diffraction method alone to accurately identify the trace amount of asbestos contained in the sample of electronic products to be tested is difficult to achieve the desired effect, so In view of the complex composition and structure of asbestos, it is difficult to accurately identify it with a single technique, and the arbitrator method relies too much on expensive instruments and equipment, and its universality is very low

Method used

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  • Polarized light microscopy-X-ray diffraction method for qualitative detection of asbestos in electronic products
  • Polarized light microscopy-X-ray diffraction method for qualitative detection of asbestos in electronic products
  • Polarized light microscopy-X-ray diffraction method for qualitative detection of asbestos in electronic products

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Embodiment Construction

[0017] The present invention will be further described below in conjunction with the accompanying drawings and specific embodiments.

[0018] A kind of polarization micro-X-ray diffraction method for qualitative detection of asbestos in electronic products, the specific steps are as follows:

[0019] Step 1. Sampling and ashing treatment. After pulverizing about 5g of the sample on the electronic product to be tested, the sample is placed in a crucible and placed in a muffle furnace. The ashing temperature is greater than 500°C to remove organic substances. The ashing treatment is specific Ashing at 450°C±10°C for 1h.

[0020] Step 2, sample sieving. After the ashed electronic product sample is cooled to room temperature in a desiccator, it is ground in an agate mortar and sieved through a metal sieve with a pore size of 425 μm to 500 μm.

[0021] Step 3: Take a sample to make a specimen, weigh 20 mg of the sieved electronic product sample, place it in a 100 mL Erlenmeyer fla...

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Abstract

The invention relates to a polarized light microscopy-X-ray diffraction method for qualitative detection of asbestos in electronic products. The method combines X-ray diffraction and polarized light microscopy observation. By means of observation of a polarized light microscopy, the optical properties of a sample in oil with different refractive indexes are considered, and the asbestos type is preliminarily identified; compared with the separately used X-ray diffraction method, the polarized light microscopy-X-ray diffraction method enables diffraction observation to be targeted, and is accurate in results and good in reproducibility. The method can be used for accurately identifying the trace amount of asbestos contained in a to-be-tested sample of an electronic product, is suitable for the inspection of the asbestos in the various electronic products, and can effectively avoid asbestos hazard and trade risks of the electronic products.

Description

technical field [0001] The invention relates to the technical field of identification of asbestos materials, in particular to a qualitative detection method for asbestos in electronic products. Background technique [0002] It is generally believed that the fiber is dust with a ratio of aspect ratio > 3:1. Asbestos is fibrous and is a general term for natural fibrous siliceous minerals. It is usually divided into two categories: chrysotile and amphibole. Scientific research shows that asbestos is harmful to the environment and human health. The International Organization for Research on Cancer (IARC) has announced that asbestos is a class A carcinogen. Many multinational companies such as SONY, DELL, Sharp, IBM, etc. have also expressly banned their products or raw materials use of asbestos. The methods currently used to detect asbestos in products mainly include: phase contrast microscopy, polarizing microscopy, scanning electron microscopy analysis, transmission elect...

Claims

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Application Information

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IPC IPC(8): G01N23/2005G01N21/84
CPCG01N21/84G01N23/2005G01N2021/845G01N2223/05G01N2223/1016
Inventor 王宏伟陶自强马强夏德富苏宏伟肖海清白桦胡斌
Owner CHINESE ACAD OF INSPECTION & QUARANTINE
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