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Preparation method of washed-black clay glazed brick green body

The technology of glazed tile and black nib is applied in the field of preparation of washed black nii glazed tile body, which can solve the problems that the glazed tile green body is difficult to achieve high drying strength and flexural strength, reduces the ball milling effect, increases the reject rate, and the like, To achieve the effect of good dispersion, short ball milling time and reduced dosage

Active Publication Date: 2018-09-28
FOSHAN SHI WAN YING BRAND CERAMICS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Through step-by-step ball milling, although it can save ball milling time, reduce power consumption, and reduce production costs, since clay is a soft material, it is still unavoidable that the clay wraps the hard material during the ball milling process, and the clay will still adhere to the grinding surface. On the ball, the effect of ball milling is reduced, and it is unavoidable to avoid stratification and agglomeration of hard and soft materials due to differences in density and particle size during the drying process of the secondary mud
[0008] To sum up, in the prior art, in the process of preparing glazed brick body by using black nib as a raw material, due to the special properties of washed black ni, it is difficult to disperse in the ball mill slurry, and it cannot be mixed evenly with other hard materials. , even if the washed black tile itself has a high viscosity and is a good plastic raw material, due to the existence of local defects, it is difficult for the glazed brick body prepared by it to achieve high dry strength and flexural strength, resulting in an increase in the reject rate during processing

Method used

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  • Preparation method of washed-black clay glazed brick green body
  • Preparation method of washed-black clay glazed brick green body

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] Embodiment 1: Weigh the raw materials according to the following mass percentages: 10% of Dongyuan washed black clay, 13% of potassium sodium stone powder, 12% of Xingning high-alumina potassium sand, 28% of high-alumina sand, and 5% of wollastonite , lime 10%, Longtian sand 22%, mix them in a rotary mixer; then add a certain amount of water, and at the same time add a mass fraction of 10% of the total weight of glazed brick body raw materials to be 10wt% polyvinyl alcohol solution , sent to a ball mill for ball milling, and then sieved to remove iron; the glazed brick body raw material after iron removal was spray-dried to obtain brick body powder; the brick body powder was pressed and formed, and then dried at 140°C After 90 minutes, the adobe was prepared, and then bisque fired at 1050°C for 40 minutes to obtain the first-fired biscuit for subsequent glazing treatment. After measurement, the dry strength of the glazed brick body is 1.41MPa, and the flexural strength ...

Embodiment 2

[0036]Embodiment 2: Weigh the raw materials according to the following mass percentages: 14% of Dongyuan washed black stone powder, 18% of potassium sodium stone powder, 17% of Xingning high-alumina potassium sand, 23% of high-alumina sand, and 4% of wollastonite , Lime 7%, Longtian sand 17%, it is mixed in the rotary mixer; Then add a certain amount of water, and add 8% of the total weight of the raw material of the glazed brick body at the same time, the mass fraction is 8wt% polyvinyl alcohol The solution is sent to a ball mill for ball milling, and then sieved to remove iron; the glazed brick body raw material after iron removal is spray-dried to obtain brick body powder; the brick body powder is pressed and formed, and then Dry for 100 minutes to make adobe, and then biscuit firing at 1080°C for 50 minutes to obtain the first-fired biscuit for subsequent glazing treatment. After measurement, the dry strength of the glazed tile body is 1.45MPa, and the flexural strength of...

Embodiment 3

[0037] Embodiment 3: Weigh the raw materials according to the following mass percentages: 15% of Dongyuan washed black clay, 23% of potassium sodium stone powder, 22% of Xingning high-alumina potassium sand, 20% of high-alumina sand, and 2% of wollastonite , Lime 5%, Longtian sand 13%, mix it in a rotary mixer; then add a certain amount of water, and add 5% of the total weight of the raw materials of the glazed brick body at the same time. The mass fraction is 5wt% polyvinyl alcohol The solution is sent to a ball mill for ball milling, and then sieved to remove iron; the glazed brick body raw material after iron removal is spray-dried to obtain brick body powder; the brick body powder is pressed and formed, and then Dry for 120 minutes to make adobe, and then biscuit firing at 1100°C for 60 minutes to obtain the first-fired biscuit for subsequent glazing treatment. After measurement, the dry strength of the glazed tile body is 1.48MPa, and the flexural strength of the green bo...

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Abstract

The invention provides a preparation method of a washed-black clay glazed brick green body. Local resourceful raw mineral materials of Guangdong washed-black clay, potassium-sodium stone powder, Xingning high-aluminium high-potassium sand, high-aluminium sand, wollastonite, burnt lime and Longtian sand are used, by adjusting the raw material composition proportion, the soft raw material washed-black clay and the hard raw materials are subjected to ball-milling separately, after spray drying, hydrocyclone reaction is conducted, then a polyvinyl alcohol solution is added in an atomizing and spraying mode, compression moulding and drying are conducted to prepare a brick green body, and finally, a biscuit is obtained through sintering. According to the method, ball-milling time is short, the efficiency is high, the washed-black clay is good in dispersibility and small in grain size, even mixing can be achieved by the washed-black clay and the hard raw materials, compared with a traditionalball-milling mixing working procedure, the method has the advantages that the usage of the additive polyvinyl alcohol solution can be reduced, and meanwhile, the glazed brick green body with high drying strength and rupture strength can be obtained.

Description

technical field [0001] The invention belongs to the field of building materials, in particular to a method for preparing a water-washed black glazed brick body. Background technique [0002] With the advancement of urbanization and new rural construction in the past ten years, the real estate industry has developed vigorously, and people's interior decoration grades have also been continuously improved. Glazed tiles have always been favored as a high-strength, easy-to-clean, and formaldehyde-free building decoration material. , and China has a long history and advanced technology in the development of ceramic materials, and now a large number of ceramic materials such as glazed tiles are exported abroad. [0003] In the production process of glazed tiles, clay is commonly used as its plastic raw material, and its addition amount is generally more than 20%. In order to produce high-quality glazed tiles and increase added value, high-quality clay is often used as raw material...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/18C04B35/626
CPCC04B35/18C04B35/62605C04B35/6261C04B35/62655C04B2235/3201C04B2235/3445C04B2235/3454C04B2235/3472C04B2235/349C04B2235/656C04B2235/96
Inventor 林伟袁红吴则昌林金宏肖春燕
Owner FOSHAN SHI WAN YING BRAND CERAMICS CO LTD
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