Titanium dioxide-multi-walled carbon nano-tube-polydimethylsiloxane composite functional material as well as preparation method and application thereof
A technology of polydimethylsiloxane and multi-walled carbon nanotubes, applied in chemical instruments and methods, alkali metal oxides/hydroxides, alkali metal compounds, etc., can solve the problem of large amount of nitric acid and increased work intensity , high acidity and other problems, achieve good molecular concentration and interaction, save production costs, clean and non-toxic reagents
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Embodiment 1
[0067] A titanium dioxide-multi-wall carbon nanotube-polydimethylsiloxane composite functional material, which is based on polydimethylsiloxane, and titanium dioxide-multi-wall carbon nanotube dry powder, prepared by a microfluidic method made microspheres.
[0068] Preparation method embodiment one
[0069] A preparation method of titanium dioxide / multi-walled carbon nanotubes / polydimethylsiloxane composite functional material, comprising the steps of:
[0070]1) Acidification and oxidation treatment of multi-walled carbon nanotubes, mixing 5g of multi-walled carbon nanotubes to a volume of 125ml with a concentration of 98% sulfuric acid kept stirring in a 250ml flask until a homogeneous solution appeared, and then added dropwise at a concentration of 30% hydrogen peroxide with a volume of 62.5ml was stirred and refluxed at 120°C for 24 hours; after the reaction, it was diluted with water until the pH returned to neutral, separated by filtration, and dried at 80°C for 2 days...
Embodiment 4
[0090] A preparation method of titanium dioxide / multi-walled carbon nanotubes / polydimethylsiloxane composite functional material, comprising the steps of:
[0091] 1) Acidification and oxidation treatment of multi-walled carbon nanotubes, mixing 5g of multi-walled carbon nanotubes to a volume of 125ml with a concentration of 98% sulfuric acid kept stirring in a 250ml flask until a homogeneous solution appeared, and then added dropwise at a concentration of 30% hydrogen peroxide with a volume of 62.5ml was stirred and refluxed at 120°C for 24 hours; after the reaction, it was diluted with water until the pH returned to neutral, separated by filtration, and dried at 80°C for 2 days to obtain acidified and oxidized polysaccharides. walled carbon nanotubes;
[0092] 2) Mix 35 mg of acidified and oxidized multi-walled carbon nanotubes with 0.5 wt % 2 ml of sodium p-dodecylbenzenesulfonate aqueous solution, sonicate for 12 hours, then pour into 20 ml of isopropanol and stir evenly f...
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