Method for increasing dyeing depth of cochineal of cotton fabric
A technology of cochineal and dyeing depth, which is applied in the field of textile dyeing, can solve the problem that cochineal does not dye cotton cloth, and achieve the effects of increasing utilization value, increasing dyeing depth, improving quality and application efficiency
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Embodiment 1
[0024] The method for improving the depth of cotton carmine dyeing, the specific steps are as follows:
[0025] (1) Preparation of bis(3-chloro-2-hydroxypropyl)tetramethylethylenediammonium dichloride: Add 49g of 18% hydrochloric acid into a 250mL four-necked reaction flask, start stirring, and slowly dissolve the four Add 29 g of methylethylenediamine into a four-necked reaction flask, and control the temperature below 40°C. After the addition of tetramethylethylenediamine, the temperature of the reaction solution was raised to 60°C, and then 32 g of epichlorohydrin was slowly added into the four-necked reaction flask, and the addition was completed over 2.5 hours, and the temperature was kept at 60°C for 40 minutes. The product is cooled to below 40°C, and bis(3-chloro-2-hydroxypropyl)tetramethylethylenediammonium dichloride is obtained by discharging.
[0026] (2) Configure cationic modifier solution: dissolve the bis(3-chloro-2-hydroxypropyl)tetramethylethylenediammonium ...
Embodiment 2
[0032] The method for improving the depth of cotton carmine dyeing, the specific steps are as follows:
[0033] (1) Preparation of two (3-chloro-2-hydroxypropyl) tetramethylethylenediammonium dichloride: same as Example 1.
[0034] (2) Configure cationic modifier solution: dissolve the bis(3-chloro-2-hydroxypropyl)tetramethylethylenediammonium dichloride prepared in step (1) in deionized water, fully dissolve and disperse A cationic modifier solution with a concentration of 30 g / L was prepared.
[0035] (3) Cationic modification of cotton cloth: at room temperature, the cotton cloth is soaked and rolled with the cationic modifier solution once, and the liquid-carrying rate of the cotton cloth after padding is 70%, and then dried at 80°C for 8 minutes, and cooled naturally to obtain cotton cloth Improve the semi-finished product; then at room temperature, soak and roll the 8g / L sodium hydroxide solution of the improved cotton cloth obtained at room temperature; Then baked at ...
Embodiment 3
[0040] The method for improving the depth of cotton carmine dyeing, the specific steps are as follows:
[0041] (1) Preparation of two (3-chloro-2-hydroxypropyl) tetramethylethylenediammonium dichloride: same as Example 1.
[0042] (2) Configure cationic modifier solution: dissolve the bis(3-chloro-2-hydroxypropyl)tetramethylethylenediammonium dichloride prepared in step (1) in deionized water, fully dissolve and disperse A cationic modifier solution with a concentration of 20 g / L was prepared.
[0043](3) Cationic modification of cotton cloth: at room temperature, the cotton cloth is soaked and rolled with the cationic modifier solution once, and the liquid-carrying rate of the cotton cloth after padding is 90%, then dried at 80°C for 8 minutes, and cooled naturally to obtain cotton cloth Improve the semi-finished product; then at room temperature, soak and roll the obtained cotton cloth to improve the semi-finished product with 25g / L of sodium hydroxide solution. After dipp...
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