A kind of walnut green skin black hair dye and preparation method thereof
A technology of black hair dye and walnut green peel, which is applied in the field of black hair dye, can solve problems such as hidden dangers of human health, and achieve the effects of high safety, good penetration efficiency, and high reproducibility
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[0083] The present invention also provides a preparation method of the above-mentioned walnut green skin black hair dye, the preparation method comprising the following steps:
[0084] (1) Prepare hair dye I agent;
[0085] (2) Prepare hair dye II agent.
[0086] Wherein, in step (1), the penetrating agent, complexing agent and part of thickener are dissolved in deionized water; In ionized water, after stirring evenly, the hair dye I agent is obtained.
[0087] Preferably, when multiple thickeners are used, the thickener with a slow dissolution rate is preferentially dissolved, and then the thickener with a fast dissolution rate is dissolved. For example, when sodium carboxymethyl cellulose and hydroxyethyl cellulose are used as thickeners, sodium carboxymethyl cellulose can be dissolved first, and then hydroxyethyl cellulose can be dissolved.
[0088] More preferably, when dissolving the penetrating agent, complexing agent and slow dissolving thickener in deionized water, ...
Embodiment 1
[0097] Walnut green skin black hair dye prescription 1
[0098] Hair dye I agent:
[0099]
[0100]
[0101] Hair dye II agent:
[0102]
[0103] The preparation method of walnut green peel extract is:
[0104] Fresh walnut green husks were chopped into small pieces with a particle size of about 2 cm. In 2% sodium hydroxide solution, ultrasonically extracted for 0.5 h according to the mass ratio of solid to liquid of 1:2.5, the ultrasonic frequency was 80KHz, and the power was 600W.
[0105] Preparation:
[0106] Add L-cysteine, EDTA-2Na, sodium thiosulfate and sodium carboxymethylcellulose into 50 mL of deionized water, heat at 85°C for 5 min, and stir to dissolve. After the solution is cooled to room temperature, walnut green husk extract, tea polyphenols, ascorbic acid, and hydroxyethyl cellulose are added into the solution, stirred to dissolve, and mixed uniformly to obtain the hair dye I agent.
[0107] Add ferrous sulfate heptahydrate into 10 mL of deionized...
Embodiment 2
[0109] Walnut green skin black hair dye prescription 2
[0110] Hair dye I agent:
[0111]
[0112]
[0113] Hair dye II agent:
[0114]
[0115] The preparation method of walnut green peel extract is:
[0116] Fresh walnut green husks were chopped into small pieces with a particle size of about 1.5 cm. In 4% sodium hydroxide solution, ultrasonic extraction was carried out for 0.5 h at a solid-liquid mass ratio of 1:1.5. The ultrasonic frequency was 80KHz and the power was 800W.
[0117] Preparation:
[0118] Add L-cysteine, EDTA-2Na, sodium thiosulfate and sodium carboxymethylcellulose into deionized water, heat at 60°C for 8 minutes, and stir to dissolve. After the solution is cooled to room temperature, walnut green husk extract, tea polyphenols, ascorbic acid, and hydroxyethyl cellulose are added into the solution, stirred to dissolve, and mixed uniformly to obtain the hair dye I agent.
[0119] Add ferrous sulfate heptahydrate into 15 mL of deionized water and ...
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