Preparation method of poultry plasma protein
A technology of plasma protein and plasma protein powder, which is applied in the field of plasma protein processing, can solve the problems of limiting the industrialization and application range of plasma protein, poor flexibility of plasma protein structure, and reduced overall solubility, so as to improve the overall solubility and reduce particle size. The effect of small and soft shaking conditions
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[0032] The invention provides a method for preparing poultry plasma protein, comprising the steps of:
[0033] Step 1, taking poultry blood, and obtaining plasma liquid through processing;
[0034] Step 2: Perform ultrasonic treatment on the plasma liquid, the ultrasonic power is 100-300W, and the ultrasonic time is 10-30min;
[0035] Step 3: Adjust the pH of the ultrasonically treated plasma to 8.5-9.5, and then perform ultrafiltration at an ultrafiltration pressure of 0.3-0.6 MPa, with a molecular weight cut-off of 5,000-10,000 Da of plasma, and an ultrafiltration cycle time of 10-100 Da. 30min;
[0036] Step 4, drying the plasma liquid obtained in Step 3 to obtain poultry plasma protein powder.
[0037] The invention conducts ultrasonic treatment on plasma liquid, which can effectively destroy the highly folded and compact structure of plasma protein molecules, change the flexibility of plasma protein structure, improve its overall solubility, have good emulsification and...
Embodiment 1
[0055] A method for preparing poultry plasma protein, comprising the steps of:
[0056] (1) Blood collection: fresh and healthy poultry blood is collected with a vacuum blood collection knife, and a compound anticoagulant is added. The final concentration of the agent in the blood is 0.8g / mL, mix well, and store under refrigerated conditions.
[0057] (2) Separation at rest: the blood was left at rest at 5° C., and centrifuged at 2500 g for 15 minutes to obtain the upper layer of plasma.
[0058] (3) Ultrasonic treatment is performed on the upper plasma liquid mixture, the ultrasonic power is 200W, and the ultrasonic time is 20min;
[0059] (4) Use NaOH / NaHCO 3 Adjust the pH of plasma liquid to 9.0, 0.45MPa ultrafiltration to the end, desalination, plasma liquid with a molecular weight cut-off of 7500Da, ultrafiltration cycle time is 20min.
[0060] (5) Drying: Pre-freeze the treated plasma liquid at -35°C, and freeze-dry at -45°C for 60 hours in a cold trap to obtain poult...
Embodiment 2
[0062] A method for preparing poultry plasma protein, comprising the steps of:
[0063] (1) Blood collection: fresh and healthy poultry blood is collected with a vacuum blood sampling knife, and a compound anticoagulant is added, which includes sodium citrate, sodium citrate, and heparin with a mass ratio of 1:1:1, so that The final concentration of the agent in the blood is 0.6g / mL, mix well, and store under refrigerated conditions.
[0064] (2) Static separation: the blood was allowed to stand at 4°C, and centrifuged at 2000g for 10 minutes to obtain the upper layer of plasma.
[0065] (3) Ultrasonic treatment is performed on the upper plasma liquid mixture, the ultrasonic power is 100W, and the ultrasonic time is 10min;
[0066] (4) Use NaOH / NaHCO 3 Adjust the pH of the plasma solution to 8.5, 0.3MPa ultrafiltration to the end, desalination, the plasma solution with a molecular weight cut-off of 5000Da, and an ultrafiltration cycle time of 10 minutes.
[0067] (5) Drying...
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