Preparation method of core-shell structure particle reinforced aluminum matrix composite

A particle-reinforced aluminum and composite material technology, applied in metal processing equipment, coating, transportation and packaging, etc., can solve the problems of high particle brittleness, composite material strength and plasticity decline, etc., achieve high elastic modulus, increase strength, Effect of suppressing crack growth

Active Publication Date: 2018-11-16
BEIJING INSTITUTE OF TECHNOLOGYGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The method overcomes the disadvantages of high brittleness of titanium-aluminum intermetallic compound particles, abnormal growth at higher temperatures, and coarsening of matrix grains, which cause the strength and plasticity of the composite material to decrease.

Method used

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  • Preparation method of core-shell structure particle reinforced aluminum matrix composite
  • Preparation method of core-shell structure particle reinforced aluminum matrix composite
  • Preparation method of core-shell structure particle reinforced aluminum matrix composite

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] A method for preparing a core-shell structure particle reinforced aluminum matrix composite material, the method steps are as follows:

[0051] (1) Add 0.15g Ti powder and 14.85g Al powder into the ball mill tank of SM-QB planetary ball mill, and add grinding balls and excess absolute ethanol according to the ball-to-material ratio of 0.5:1; at a speed of 600r / min , ball milled for 0.5h, and mixed evenly to obtain a mixed slurry; the mixed slurry was poured into a vacuum rotary evaporator, and the rotation speed was 100r / min, and the temperature of the water bath was 80°C, and then steamed for 0.2h, and after the ball milling medium was volatilized, the obtained Mixing the powder precursors; putting the mixed powder precursors into an electrothermal constant-temperature blast drying oven, and drying at 60° C. for 1 hour to obtain mixed powders.

[0052] Wherein, the grinding ball is composed of a large agate ball and a small agate ball with a mass ratio of 0.1:1, the di...

Embodiment 2

[0079] A method for preparing a core-shell structure particle reinforced aluminum matrix composite material, the method steps are as follows:

[0080] (1) Add 2.4g Ti powder and 17.6g Al powder into the ball mill tank of SM-QB planetary ball mill, and add grinding balls and excess absolute ethanol according to the ball-to-material ratio of 4:1; at a speed of 300r / min , ball milled for 2 hours, and mixed uniformly to obtain a mixed slurry; the mixed slurry was poured into a vacuum rotary evaporator, and the rotating speed was 40r / min, and the temperature of the water bath was 70°C, and then steamed for 0.5h, and the mixed slurry was obtained after the volatilization of the ball milling medium was completed. Powder precursor: put the mixed powder precursor into an electric heating constant temperature blast drying oven, and dry at 30°C for 0.5h to obtain a mixed powder.

[0081] Wherein, the grinding ball is composed of a large agate ball and a small agate ball with a mass ratio...

Embodiment 3

[0108] A method for preparing a core-shell structure particle reinforced aluminum matrix composite material, the method steps are as follows:

[0109] (1) Add 4.5g Ti powder and 10.5g 7075 aluminum alloy powder into the ball mill tank of SM-QB planetary ball mill, and add grinding balls and excess absolute ethanol according to the ball-to-material ratio of 10:1; at 150r / min Under the speed of rotation, ball mill for 2 hours, and mix evenly to obtain a mixed slurry; pour the mixed slurry into a vacuum rotary evaporator, turn the steam at a rotation speed of 40r / min and a water bath temperature of 70°C for 2 hours, and obtain Mixing powder precursors; putting the mixed powder precursors into an electrothermal constant temperature blast drying oven, and drying at 30° C. for 0.5 h to obtain mixed powders.

[0110] Wherein, the grinding ball is composed of a large agate ball and a small agate ball with a mass ratio of 10:1, the diameter of the large agate ball is 30mm, and the diam...

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Abstract

The invention relates to a preparation method of a core-shell structure particle reinforced aluminum matrix composite, and belongs to the field of metal matrix composites. The method combines in-situreaction, spark plasma sintering and hot rolling technologies. The method includes utilizing the advantages of the spark plasma sintering of high sintering efficiency and controllable extra pressure and sintering atmosphere and controlling the outer layer of titanium particles to react with a surrounding aluminum matrix to prepare the core-shell structure particle reinforced aluminum matrix composite at low sintering temperature; then conducting rolling to further reducing the porosity in a microstructure and improve the strength and the plasticity of the composite. According to the method, the shortcomings of high brittleness of titanium aluminum intermetallic compound particles, abnormal growth at higher temperature and reduction of the strength and the plasticity of the composite causedby matrix grain coarsening are overcome.

Description

technical field [0001] The invention relates to a preparation method of a core-shell structure particle reinforced aluminum matrix composite material, belonging to the field of metal matrix composite materials. Background technique [0002] Discontinuous phase reinforced aluminum matrix composites (DRAMCs) have low density, thermal expansion coefficient, high specific stiffness, specific strength, wear resistance, excellent dimensional stability and medium temperature mechanical properties, and are widely used, such as aerospace , automotive equipment, military, etc., almost involve all sectors of the national economy and various fields of modern technology, and play an important role in promoting the development of industry and the improvement of productivity. [0003] Titanium-aluminum intermetallic particles, such as Al 3 Ti, with low density (3.4g / cm 3 ), high melting point (1613K), oxidation resistance, high modulus (216GPa), etc., and can be formed by the in-situ rea...

Claims

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Application Information

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IPC IPC(8): B22F3/105B22F3/18B22F9/04B22F1/02
CPCB22F3/105B22F3/18B22F9/04B22F2003/185B22F2009/043B22F2003/1051B22F2998/10B22F1/17
Inventor张朝晖胡正阳程兴旺王富耻宋奇尹世攀王浩王虎
OwnerBEIJING INSTITUTE OF TECHNOLOGYGY