A preparation method of high-performance carbon-silicon composite material for lithium batteries

A composite material, high-performance technology, used in nanotechnology for materials and surface science, battery electrodes, secondary batteries, etc., can solve the problems of brittleness and pulverization of carbon-silicon composite particles, and achieve good connection effect. Effect

Active Publication Date: 2021-10-22
东莞市睿丰能源科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Aiming at the problems in the prior art, the present invention provides a method for preparing a high-performance carbon-silicon composite material for lithium batteries, which solves the problems of fragility and pulverization of carbon-silicon composite particles in the prior art

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] A method for preparing a high-performance carbon-silicon composite material for lithium batteries, comprising the steps of:

[0035] Step 1, putting nano-carbon material and nano-silicon material into absolute ethanol and stirring evenly, then putting them into a ball mill at constant temperature and ball milling for 1 hour to obtain a mixed alcohol solution;

[0036] Step 2, adding hydroxypropyl cellulose to the mixed alcohol solution, stirring evenly, and ultrasonically reacting for 30 minutes to obtain a dispersion suspension;

[0037] Step 3, put the dispersed suspension into a vacuum distillation kettle for a vacuum distillation reaction for 30 minutes to obtain a viscous liquid;

[0038] Step 4, add the viscous liquid into distilled water and stir evenly, put it into a mold for gradient solidification and distillation for 3 hours, and obtain a carbon-silicon composite preform;

[0039] Step 5, adding the carbon-silicon composite preform into the reactor for gradi...

Embodiment 2

[0050] A method for preparing a high-performance carbon-silicon composite material for lithium batteries, comprising the steps of:

[0051] Step 1, put the nano-carbon material and the nano-silicon material into absolute ethanol and stir evenly, then put them into a ball mill for constant temperature ball milling for 3 hours to obtain a mixed alcohol solution;

[0052] Step 2, adding hydroxypropyl cellulose to the mixed alcohol solution, stirring evenly, and ultrasonically reacting for 60 minutes to obtain a dispersion suspension;

[0053] Step 3, put the dispersed suspension into a vacuum distillation kettle for 70 minutes of vacuum distillation to obtain a viscous liquid;

[0054] Step 4, add the viscous liquid into distilled water and stir evenly, put it into a mold for gradient solidification and distillation reaction for 6 hours, and obtain a carbon-silicon composite preform;

[0055] Step 5, adding the carbon-silicon composite preform into the reactor for gradient anaer...

Embodiment 3

[0066] A method for preparing a high-performance carbon-silicon composite material for lithium batteries, comprising the steps of:

[0067] Step 1, put the nano-carbon material and the nano-silicon material in absolute ethanol and stir evenly, then put them into a ball mill for constant temperature ball milling for 2 hours to obtain a mixed alcohol solution;

[0068] Step 2, adding hydroxypropyl cellulose to the mixed alcohol solution, stirring evenly, and ultrasonically reacting for 50 minutes to obtain a dispersion suspension;

[0069] Step 3, put the dispersed suspension into a vacuum distillation kettle for 50 minutes of vacuum distillation to obtain a viscous liquid;

[0070] Step 4, add the viscous liquid into distilled water and stir evenly, put it into a mold for gradient solidification and distillation reaction for 5 hours, and obtain a carbon-silicon composite preform;

[0071] Step 5, adding the carbon-silicon composite preform into the reactor for gradient anaerob...

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PUM

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Abstract

The invention belongs to the technical field of lithium batteries, in particular to a method for preparing a high-performance carbon-silicon composite material for lithium batteries, comprising the following steps: step 1, putting nano-carbon materials and nano-silicon materials into absolute ethanol and stirring evenly , and then put it into a ball mill for constant temperature ball milling for 1-3h to obtain a mixed alcohol solution; step 2, add hydroxypropyl cellulose to the mixed alcohol solution and stir evenly, and ultrasonically react for 30-60min to obtain a dispersed suspension; step 3, Put the dispersed suspension in a vacuum distillation kettle for 30-70 minutes to obtain a viscous liquid; step 4, add the viscous liquid to distilled water and stir evenly, put it into a grinding tool for gradient solidification distillation reaction 3- 6h, to obtain the carbon-silicon composite preform; Step 5, adding the carbon-silicon composite preform to the reactor for gradient anaerobic carbonization reaction for 5‑7h, to obtain the carbon-silicon composite nanomaterial. The invention solves the problems of friability and pulverization of carbon-silicon composite particles in the prior art.

Description

technical field [0001] The invention belongs to the technical field of lithium batteries, and in particular relates to a preparation method of a high-performance carbon-silicon composite material for lithium batteries. Background technique [0002] Lithium-ion batteries are energy storage devices that have attracted much attention. In recent years, lithium-ion batteries have been widely used in portable electronic devices, and their applications in vehicles such as automobiles have also attracted much attention. [0003] The working principle of a lithium-ion battery is roughly as follows: when the battery is charged, the anode (that is, the negative electrode) absorbs lithium ions from the cathode, and absorbs electrons from the external circuit through the charging device, and releases these ions and electrons back to the cathode when the battery is discharged. The mass-specific capacity is an important parameter for anode materials because it determines the amount of lit...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01M4/36H01M4/38H01M4/587H01M4/62H01M10/0525B82Y30/00
CPCB82Y30/00H01M4/364H01M4/386H01M4/587H01M4/622H01M4/628H01M10/0525Y02E60/10
Inventor 祝良荣杨建青
Owner 东莞市睿丰能源科技有限公司
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