A preparation method of high-performance carbon-silicon composite material for lithium batteries
A composite material, high-performance technology, used in nanotechnology for materials and surface science, battery electrodes, secondary batteries, etc., can solve the problems of brittleness and pulverization of carbon-silicon composite particles, and achieve good connection effect. Effect
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Embodiment 1
[0034] A method for preparing a high-performance carbon-silicon composite material for lithium batteries, comprising the steps of:
[0035] Step 1, putting nano-carbon material and nano-silicon material into absolute ethanol and stirring evenly, then putting them into a ball mill at constant temperature and ball milling for 1 hour to obtain a mixed alcohol solution;
[0036] Step 2, adding hydroxypropyl cellulose to the mixed alcohol solution, stirring evenly, and ultrasonically reacting for 30 minutes to obtain a dispersion suspension;
[0037] Step 3, put the dispersed suspension into a vacuum distillation kettle for a vacuum distillation reaction for 30 minutes to obtain a viscous liquid;
[0038] Step 4, add the viscous liquid into distilled water and stir evenly, put it into a mold for gradient solidification and distillation for 3 hours, and obtain a carbon-silicon composite preform;
[0039] Step 5, adding the carbon-silicon composite preform into the reactor for gradi...
Embodiment 2
[0050] A method for preparing a high-performance carbon-silicon composite material for lithium batteries, comprising the steps of:
[0051] Step 1, put the nano-carbon material and the nano-silicon material into absolute ethanol and stir evenly, then put them into a ball mill for constant temperature ball milling for 3 hours to obtain a mixed alcohol solution;
[0052] Step 2, adding hydroxypropyl cellulose to the mixed alcohol solution, stirring evenly, and ultrasonically reacting for 60 minutes to obtain a dispersion suspension;
[0053] Step 3, put the dispersed suspension into a vacuum distillation kettle for 70 minutes of vacuum distillation to obtain a viscous liquid;
[0054] Step 4, add the viscous liquid into distilled water and stir evenly, put it into a mold for gradient solidification and distillation reaction for 6 hours, and obtain a carbon-silicon composite preform;
[0055] Step 5, adding the carbon-silicon composite preform into the reactor for gradient anaer...
Embodiment 3
[0066] A method for preparing a high-performance carbon-silicon composite material for lithium batteries, comprising the steps of:
[0067] Step 1, put the nano-carbon material and the nano-silicon material in absolute ethanol and stir evenly, then put them into a ball mill for constant temperature ball milling for 2 hours to obtain a mixed alcohol solution;
[0068] Step 2, adding hydroxypropyl cellulose to the mixed alcohol solution, stirring evenly, and ultrasonically reacting for 50 minutes to obtain a dispersion suspension;
[0069] Step 3, put the dispersed suspension into a vacuum distillation kettle for 50 minutes of vacuum distillation to obtain a viscous liquid;
[0070] Step 4, add the viscous liquid into distilled water and stir evenly, put it into a mold for gradient solidification and distillation reaction for 5 hours, and obtain a carbon-silicon composite preform;
[0071] Step 5, adding the carbon-silicon composite preform into the reactor for gradient anaerob...
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