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31results about How to "Good dispersion system" patented technology

Preparation method of nanometer titanium dioxide

The invention belongs to the technical field of environment-friendly materials, and particularly relates to a preparation method of nanometer titanium dioxide. The preparation method comprises the following steps: 1, adding n-butyl titanate into absolute ethanol, then adding a dispersing agent, ultrasonically dispersing till complete dissolution to obtain n-butyl titanate alcohol dispersion; 2, adding a polymer surfactant into distilled water, uniformly stirring till complete dissolution to obtain a dropping solution; 3, slowly dropwise adding the dropping solution into the n-butyl titanate alcohol solution, sealing, slightly heating while stirring for 1-3 hours to obtain a suspension; 4, placing the suspension in a reaction kettle, performing a vacuum distillation reaction for 1-3h, cooling, then filtering at low temperature to obtain a wrapped titanium dioxide precipitate; 5, adding the wrapped titanium dioxide precipitate into an aqueous ethanol solution, performing an ultrasonic reaction for 10-20min, then taking and drying at a high temperature to obtain the nanometer titanium dioxide. Through hydrolysis of the n-butyl titanate, and by virtue of the dual action of polyvinylpyrrolidone and sodium lauryl sulfate, a good dispersion system can be formed, so that agglomeration of titanium dioxide is prevented.
Owner:蒋建华

MXene and carbon nano tube synergistically modified polyurethane anticorrosive paint as well as preparation method and construction process thereof

ActiveCN114276743APrevent diffusion and penetrationGood mechanical properties and anti-corrosion propertiesPretreated surfacesAnti-corrosive paintsSilane couplingCarbon nanotube
The invention discloses an MXene and carbon nanotube synergistically modified polyurethane anti-corrosion coating as well as a preparation method and a construction process thereof, and relates to the field of anti-corrosion coatings. Comprising the following steps: S1, taking MXene nanosheets, and adding a silane coupling agent for modification to obtain functionalized MXene nanosheets; s2, dispersing the functionalized MXene nanosheets and the aminated carbon nanotubes in deionized water, and carrying out ultrasonic treatment until the functionalized MXene nanosheets and the aminated carbon nanotubes are uniformly dispersed, so as to obtain A-MXene/AMCNT dispersion liquid; and S3, adding the A-MXene/AMCNT dispersion liquid into waterborne polyurethane, and uniformly stirring, so as to obtain the MXene and carbon nanotube synergistically modified polyurethane anticorrosive coating. According to the preparation method disclosed by the invention, the MXene nanosheet can have good compatibility and relatively strong interface interaction with the WPU substrate, so that the MXene and the carbon nanotubes of the coating are uniformly dispersed in the WPU substrate, and the coating has excellent corrosion resistance and mechanical properties.
Owner:HENAN INST OF ENG

Foamed aluminum supercritical preparation method with controllable hole diameters

The invention belongs to the technical field of aluminum materials, and particularly relates to a foamed aluminum supercritical preparation method with controllable hole diameters. The method includesthe steps that 1, ethyecellulose is added into absolute ethyl alcohol for ultrasonic treatment for 5-10 min, and dispersive alcohol liquid is obtained; 2, broken aluminum skimmings are added into thedispersive alcohol liquid to be stirred for 20-50 min, and suspended alcohol liquid is obtained; 3, supercritical carbon dioxide fluid is flushed into the suspended alcohol liquid for a constant-pressure microwave reaction for 1-3 h, and mixed liquid is obtained after settling is completed; 4, the mixed liquid is put in a metal mold for a heating constant-pressure reaction for 1-3 h and a slow constant-temperature pressure relief reaction for 2-4 h, cooling is carried out after nitrogen purging, and a foamed aluminum precursor is obtained; and 5, the foamed aluminum precursor is subjected toan illumination decomposition reaction for 2-4 h, and a foamed aluminum material is obtained. The problems that structural parameters cannot be controlled or adjusted at will are completely solved; the preparation method is simple, batched production is facilitated, and the production cost is low; and the prepared foamed aluminum has a stable and uniform pore structure, and the pore controllability is improved.
Owner:SHAOXING UNIVERSITY

Environment-friendly guiding material

The invention disclose an environment-friendly guiding material. The environment-friendly guiding material comprises, by weight, 28 to 30 parts of kaolin pulp fine material, 13 to 15 parts of polyethylene resin, 13 to 15 parts of phenolic resin, 10 to 13 parts of magnesium oxide, 16 to 18 parts of fly ash, 10 to 14 parts of ceramic powder, 10 to 14 parts of gypsum powder, 12 to 17 parts of wood chip, 16 to 21 parts of vegetable fiber, 8 to 10 parts of polyethylene glycol, 12 to 15 parts of a toughening filling material, 9 to 11 parts of an anti-oxidant, 3 to 6 parts of an expanding aid, and 13to 15 parts of water. A preparation method comprises following steps: a, fly ash, gypsum powder, wood chip, and water are mixed, an obtained mixture is introduced into a material mixing machine for uniform stirring, kaolin pulp fine material and the expanding aid are added, an obtained mixed material is heated to 72 to 74 DEG C, is stirred for 16 to 18min at a rotating speed of 200 to 220r/min, and is cooled to normal temperature so as to obtain a mixture 1. The preparation method is simple; deformation is not easily caused under pressing; a plurality of domestic waste and industrial waste are adopted; low carbon green environment protection is achieved; the environment-friendly guiding material can be widely used in the field of building material; the using rate is increased; the obtained environment-friendly guiding material is light in mass, high in compression resistance, and excellent in sound insulation thermal insulation effect.
Owner:王旭

A supercritical preparation method of aluminum foam with controllable pore size

The invention belongs to the technical field of aluminum materials, and specifically relates to a supercritical preparation method of aluminum foam with controllable pore size, comprising: step 1, adding ethyl cellulose to absolute ethanol and ultrasonicating for 5-10 minutes to obtain a dispersed alcohol solution; step 2. Add crushed aluminum scraps to the dispersing alcohol solution and stir for 20-50 minutes to obtain a suspension alcohol solution; step 3, pour supercritical carbon dioxide fluid into the suspension alcohol solution, react with microwave at constant pressure for 1-3 hours, and obtain Mixed solution; step 4, put the mixed solution into a metal mold for heating and constant pressure reaction for 1-3h, then slowly constant temperature and pressure relief reaction for 2-4h, and use nitrogen purge to cool to obtain the foamed aluminum precursor; step 5, to foam The aluminum precursor is decomposed by light for 2-4 hours to obtain foamed aluminum material. The invention thoroughly solves the problem that the structural parameters cannot be controlled and adjusted arbitrarily; the preparation method is simple, it is beneficial to mass production, and the production cost is low; the prepared foamed aluminum has a stable and uniform pore structure, which improves the controllability of the pores.
Owner:SHAOXING UNIVERSITY

A kind of preparation method of hollow aluminum oxide microsphere

The invention discloses a preparation method of hollow type alumina microspheres. The method comprises the steps that step 1, polyvinyl alcohol is added into deionized water, ultrasonically stirred until completely dissolved to obtain dispersed alcohol liquid; step 2, polylactic acid powder and a curing agent are added into a dispersed solution to conduct microwave reaction for 30 to 60 minutes, and then the mixture is added to a mold to rapidly reduce the temperature to obtain macromolecule spherical particles; step 3, ammonium aluminum carbonate hydroxide and polyvinylpyrrolidone are added into absolute ethanol to be stirred uniformly, and then uniformly coated on the surfaces of the macromolecule spherical particles, and inorganic-organic spherical particles are obtained; step 4, the inorganic-organic spherical particles are placed in a reaction kettle and heated and pressurized for 3 to 5 hours to obtain solidified spherical particles; step 5, the solidified spherical particles areplaced in a methanol reaction solution, micro-current electrolysis is carried out for 3 to 5 hours, after the reaction is completed, the solidified spherical particles are taken out for washing and drying to obtain the hollow type alumina microspheres. The preparation method of the hollow type alumina microspheres solves a problem that the preparation of inorganic hollow spheres is difficult, thepreparation method is simple and rapid, the structure is stable, and a large specific surface area is provided.
Owner:陕西瑞科新材料股份有限公司

High-fluidity ultra-high molecular weight polyethylene wear-resistant plate and preparation method thereof

The invention relates to the field of high polymer materials, and particularly discloses a high-fluidity ultra-high molecular weight polyethylene wear-resistant plate and a preparation method thereof. The high-fluidity ultra-high molecular weight polyethylene wear-resistant plate comprises the following substances in parts by weight: 20-50 parts of an ultra-high molecular weight polyethylene diaphragm plate, 18-30 parts of polyamide, 3-5 parts of paraffin oil and 2-3 parts of a functional additive. After the ultra-high molecular weight polyethylene diaphragm plate is recycled, polyamide is adopted to replace an oily material adopted in a traditional diaphragm plate, so that on one hand, the flowing property of the ultra-high molecular weight polyethylene material is effectively improved, and the ultra-high molecular weight polyethylene material is convenient to process and extrude; on the other hand, due to the good crystallization property and wear resistance of polyethylene, polyethylene is added into the ultra-high molecular weight polyethylene material, so that the wear resistance of the composite material can be improved, and the defects of poor processability and wear resistance of the recycled ultra-high molecular weight polyethylene diaphragm plate after no oily substance is added are effectively overcome.
Owner:常州利尔德通新材料科技有限公司
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