Reactive normal temperature flame retardant asphalt and its preparation method and application
A flame retardant asphalt, reactive technology, used in building insulation materials, building components, buildings, etc., can solve the problems of flame retardant heating failure, poor performance of emulsified normal temperature flame retardant asphalt mixture, etc., and achieve excellent flame retardancy. , Solve the effect of heating failure
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[0036] The second aspect of the present invention provides the preparation method of the reactive type normal temperature flame retardant asphalt of the present invention (sometimes referred to simply as "the method of the present invention" in the present invention), which comprises sequentially adding a prescribed amount of reactive solvent, Steps for water-based epoxy resin, unsaturated polyester resin, coupling agent and flame retardant.
[0037] The step (1) of the present invention is to effectively dissolve the asphalt so that it has good fluidity at normal temperature. Specifically, it refers to heating 50-60 parts by weight of asphalt to 135-150 °C, adding 20-30 parts by weight of a reactive solvent, stirring at the first stirring speed for 5-10 minutes, and then continuing to stir at the second stirring speed for 1 -10min, a mixed solution was obtained. In this step (1), it is preferred to heat to 135-150°C, preferably 140-145°C. Usually stir 5-10min under the slow...
Embodiment 1
[0044] The preparation of the reaction type normal temperature flame retardant asphalt of the present embodiment is as follows:
[0045] (1) Weigh 50 parts of petroleum base asphalt, 5 parts of water-based epoxy resin, 10 parts of unsaturated polyester resin (7901), 25 parts of reactive solvent, and 15 parts of n-dodecyl triethoxysilane by weight , 8 parts of flame retardant, spare.
[0046] The raw material of the flame retardant is composed of 30 parts by weight of chlorinated paraffin, 20 parts by weight of magnesium hydroxide, 10 parts by weight of aluminum hydroxide and 20 parts by weight of zinc borate, and the above raw materials are mixed at 60 °C and stirred evenly at 30 rpm get. The reactive solvent is obtained by weighing and mixing raw materials according to the formula of 20 parts by weight of oleic acid, 6 parts by weight of dodecyl dimethyl betaine and 4 parts by weight of tris-(dimethylaminomethyl)phenol polymer.
[0047] (2) Heat the petroleum-based asphalt ...
Embodiment 2
[0055] The preparation of the reaction type normal temperature flame retardant asphalt of the present embodiment is as follows:
[0056] (1) Weigh 50 parts of petroleum-based asphalt, 5 parts of water-based epoxy resin, 10 parts of unsaturated polyester resin (bisphenol A type unsaturated polyester), 25 parts of reactive solvent, n-dodecyl 15 parts of triethoxysilane, 8 parts of flame retardant, set aside.
[0057] The raw material of the flame retardant is composed of 25 parts by weight of chlorinated paraffin, 25 parts by weight of magnesium hydroxide, 8 parts by weight of aluminum hydroxide and 15 parts by weight of zinc borate, and the above raw materials are mixed at 60 ° C and stirred at 30 rpm get. The reactive solvent is obtained by weighing and mixing raw materials according to the formula of 20 parts by weight of oleic acid, 6 parts by weight of dodecyl dimethyl betaine and 4 parts by weight of tris-(dimethylaminomethyl)phenol polymer.
[0058] (2) Heat the petrole...
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