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High and low temperature resisting type trimesic acid synthetic ester plasticizer and preparation method thereof

A technology of trimesic acid and plasticizer, applied in the field of plastic additives, can solve the problem that plasticizers cannot have both high temperature resistance and low temperature resistance, and achieve low extraction resistance, improve high temperature resistance, and improve low temperature resistance. performance effect

Active Publication Date: 2018-12-21
安徽泰达新材料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] For this reason, the technical problem to be solved by the present invention is to provide a high-temperature-resistant and low-temperature-resistant trimesic acid synthetic ester plasticizer to solve the problem that plasticizers in the prior art cannot have both high-temperature resistance and low-temperature resistance

Method used

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  • High and low temperature resisting type trimesic acid synthetic ester plasticizer and preparation method thereof

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Embodiment 1

[0034] The high- and low-temperature-resistant trimesic acid synthetic ester plasticizer described in this embodiment includes the following raw material components in molar percentages based on the total amount of raw materials used to prepare the randomized plasticizer:

[0035] Trimellitic acid 25mol;

[0036] Pinacol 10mol;

[0037] Isooctyl alcohol 30mol;

[0038] 2-Ethyl hydroxyacetate 10mol;

[0039] 2-perfluorooctyl ethanol 15mol;

[0040] Xylene 10%mol;

[0041] Zinc fluoride borate 0.3mol.

[0042] The preparation method of the high and low temperature resistant type trimesic acid synthetic ester plasticizer described in this embodiment comprises the following steps:

[0043] (1) The trimesic acid, pinacol, xylene, and catalysts of selected molar amounts are added to the reactor, fully mixed and then heated to 130-150°C for water separation and esterification;

[0044] (2) Stop heating when the acid value drops below 450mgKOH / g, and add isooctyl alcohol, 2-hydr...

Embodiment 2

[0049] The high- and low-temperature-resistant trimesic acid synthetic ester plasticizer described in this embodiment, based on the total amount of raw materials for the preparation of the random increaser, includes the following raw material components in molar percentages:

[0050] Trimellitic acid 20mol;

[0051] Pinacol 15mol;

[0052] Isooctyl alcohol 20mol;

[0053] 2-Ethyl hydroxyacetate 18mol;

[0054] 2-perfluorooctyl ethanol 12mol;

[0055] Xylene 15%mol;

[0056] Zinc fluoride borate 0.2mol.

[0057] The preparation method of the high and low temperature resistant trimesic acid synthetic ester plasticizer described in this embodiment comprises the following steps:

[0058] (1) Add the trimesic acid, pinacol, xylene, and catalyst in selected molar amounts into the reactor, mix thoroughly and heat to 130-150° C. to carry out the water-dividing esterification reaction;

[0059] (2) Stop heating when the acid value drops below 450mgKOH / g, and add selected molar am...

Embodiment 3

[0064] The high- and low-temperature-resistant trimesic acid synthetic ester plasticizer described in this embodiment includes the following raw material components in molar percentages based on the total amount of raw materials used to prepare the randomized plasticizer:

[0065] Trimellitic acid 35mol;

[0066] Pinacol 6mol;

[0067] Isooctyl alcohol 26mol;

[0068] 2-Ethyl hydroxyacetate 8mol;

[0069] 2-perfluorooctyl ethanol 20mol;

[0070] Xylene 5%mol;

[0071] Zinc borofluorate 0.5mol.

[0072] The preparation method of the high and low temperature resistant trimesic acid synthetic ester plasticizer described in this embodiment comprises the following steps:

[0073] (1) The trimesic acid, pinacol, xylene, and catalysts of selected molar amounts are added to the reactor, fully mixed and then heated to 130-150°C for water separation and esterification;

[0074] (2) Stop heating when the acid value drops below 450mgKOH / g, and add selected molar amounts of isooctyl ...

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Abstract

The invention belongs to the technical field of plastic additives and specifically relates to a high and low temperature resisting type trimesic acid synthetic ester plasticizer and further disclosesa synthesizing method of the plasticizer and application of the plasticizer in the field of plastic processing. The trimesic acid synthetic ester plasticizer disclosed by the invention is prepared from the raw materials of trimesic acid, pinacol, isooctyl alcohol, 2-ethyl glycolate, 2-perfluorooctyl ethanol and xylene. Under the premise that excellent plasticity of a product is ensured, low temperature resistance and high temperature resistance of the product are effectively improved, and the high temperature resistance of the product can reach 160 DEG C; compared with an existing phthalate plasticizer, the plasticizer product disclosed by the invention has a relatively-large molecule structure, low extraction resistance of the product is effectively ensured, and the advantage of more stability is achieved.

Description

technical field [0001] The invention belongs to the technical field of plastic additives, in particular to a trimesic acid synthetic ester plasticizer with excellent high and low temperature resistance, and further discloses its synthesis method and its application in the field of plastic processing. Background technique [0002] Plasticizer, also known as plasticizer in general, is a polymer material additive widely used in industry, and it is also the largest additive variety in the modern plastics industry. Adding it to the resin in a certain proportion can change the properties of the resin, such as increasing the flexibility of the plastic, improving the temperature resistance, improving the usability of plastic products at low temperatures, reducing the viscosity of the molten material, and making the resin easy to process and shape, etc. , especially plays a decisive role in promoting the development of the plastics industry, especially the polyvinyl chloride industry...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C67/08C07C69/78C08K5/12C08L27/06
CPCC07C67/08C07C69/78C08K5/12C08L27/06
Inventor 柯伯成柯伯留柯美松罗建立
Owner 安徽泰达新材料股份有限公司
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