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Deepening agent composition and preparation method thereof

A technology of a composition and a deepening agent, applied in the field of textile printing and dyeing, can solve the problems of high price, less variety and high cost of the deepening agent, and achieve the effects of reducing the amount of reflected light, good solubility, and outstanding heat resistance

Active Publication Date: 2018-12-21
HT FINE CHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] So far, there are many literatures and products about darkening agents in China, but most of them focus on silicone resin darkening agents. The darkening rate of the darkening agent is 20% to 30%, and the darkening effect is not obvious
Foreign companies in the same industry have mastered a darkening agent for fluorine-containing resins, which has a good darkening effect, but the cost is too high, and for the confidentiality of the technology, the cost of using the domestic dyeing factory is relatively high, which will affect the dyeing factory's understanding of this kind of darkening agent. usability of the product
[0004] The darkening agents on the market are far from meeting the needs of the growing printing and dyeing process due to their high price and too few varieties, especially for dyeing deep black fabrics.

Method used

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Examples

Experimental program
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Effect test

preparation example Construction

[0025] In one embodiment, the preparation method of the hyperbranched polysiloxane of the epoxy group comprises the following steps: uniformly mixing distilled water with the siloxane containing the epoxy group, adding the solvent absolute ethanol, and then Slowly add the catalyst dropwise under stirring condition; after the dropwise addition, raise the temperature to 50-60°C, keep the temperature for 4-7h, wash and dry to obtain the epoxy group-containing hyperbranched polysiloxane; the distilled water and the ring-containing The weight ratio of the siloxane of the oxygen group is 1: (0.8-1.2); the weight ratio of the dehydrated alcohol to the siloxane containing the epoxy group is 1: (0.1-0.4); the The weight ratio of the catalyst to the epoxy group-containing siloxane is (0.0001-0.0003): 1; the catalyst is selected from hydrochloric acid, sulfuric acid, p-toluenesulfonic acid, tetramethylammonium hydroxide, tetraethylhydrogen One of ammonium oxide, sodium hydroxide and pota...

Embodiment 1

[0064] The raw materials for the preparation of the darkening agent composition include hyperbranched amino silicone oil and modified chitosan; the weight ratio of the hyperbranched amino silicone oil to the modified chitosan is 1:0.08; the hyperbranched amino silicone oil The preparation raw materials include hyperbranched polysiloxane containing epoxy groups, polyether amines, and lactones, and the hyperbranched polysiloxane of epoxy groups in the preparation raw materials of the hyperbranched amino silicone oil is combined with the The molar ratio of polyetheramine and the lactone is 1:2.4:1.2; the siloxane containing epoxy group described in the preparation method of the hyperbranched polysiloxane of the epoxy group is (3-ring Oxypropoxypropyl) dimethylethoxysilane; the polyetheramine is polyetheramine D400; the lactone is β-butyrolactone and L-ribonic acid-1,4-lactone, so The molar ratio of said β-butyrolactone and said L-ribonic acid-1,4-lactone is 1:0.32; said modified ...

Embodiment 2

[0077] The raw materials for the preparation of the darkening agent composition include hyperbranched amino silicone oil and modified chitosan; the weight ratio of the hyperbranched amino silicone oil to the modified chitosan is 1:0.01; the hyperbranched amino silicone oil The preparation raw materials include hyperbranched polysiloxane containing epoxy groups, polyether amines, and lactones, and the hyperbranched polysiloxane of epoxy groups in the preparation raw materials of the hyperbranched amino silicone oil is combined with the The molar ratio of polyetheramine and the lactone is 1:2.4:1.2; the siloxane containing epoxy group described in the preparation method of the hyperbranched polysiloxane of the epoxy group is (3-ring Oxypropoxypropyl) dimethylethoxysilane; the polyetheramine is polyetheramine D400; the lactone is β-butyrolactone and L-ribonic acid-1,4-lactone, so The molar ratio of said β-butyrolactone and said L-ribonic acid-1,4-lactone is 1:0.32; said modified ...

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Abstract

The invention provides a deepening agent composition. Preparation raw materials for the deepening agent composition comprise hyperbranched amino silicon oil and modified chitosan in a weight ratio of1 to (0.01-0.2).

Description

technical field [0001] The invention belongs to the technical field of textile printing and dyeing, in particular, the invention relates to a darkening agent composition and a preparation method thereof. Background technique [0002] With the development of the economy, the requirements for environmental protection at home and abroad are getting higher and higher, and the production cost of the dyeing factory is increasing. It is imperative to reduce the amount of dye to reduce the cost. In order to achieve the same dyeing depth, darkening agents came into being. Especially the post-finishing darkening agent has the most practical value. [0003] So far, there are many literatures and products about darkening agents in China, but most of them focus on silicone resin darkening agents. The darkening rate of the darkening agent is 20% to 30%, and the darkening effect is not obvious. Foreign companies in the same industry have mastered a darkening agent for fluorine-containing...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/52D06P1/48C08G77/46C08B37/08
CPCC08B37/003C08G77/46D06P1/48D06P1/5292
Inventor 程文静刘锦凡郑靖宇汤金伟方伟洪
Owner HT FINE CHEM CO LTD
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