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Quality control method of traditional Chinese medicine Zhenlian immunity-boosting oral solution

A quality inspection method and oral liquid technology, which can be used in measurement devices, instruments, scientific instruments, etc., can solve the problems of mixed product quality and inability to guarantee the effect of products, and achieve quality stability, quality improvement, and good accuracy. Effect

Inactive Publication Date: 2018-12-21
SHIJIAZHUANG WEIERLI ANIMAL PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Moreover, there are currently many manufacturers of traditional Chinese medicine compound preparations, resulting in mixed product quality, and even some companies do not feed their products according to the standard requirements, so the quality of the products cannot guarantee the effect of clinical treatment.

Method used

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  • Quality control method of traditional Chinese medicine Zhenlian immunity-boosting oral solution
  • Quality control method of traditional Chinese medicine Zhenlian immunity-boosting oral solution
  • Quality control method of traditional Chinese medicine Zhenlian immunity-boosting oral solution

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0055] Weigh 140g each of Ligustrum lucidum, Eclipta, and Epimedium, 30g of Astragalus, 15g of Burdock, and 20g of Gynostemma, add water to decoct 3 times, and the amount of water added for each decoction is 10 times the total mass of sheepskin, astragalus, arctium and gynostemma, the filtrates were combined, concentrated under reduced pressure, precipitated with ethanol with a mass concentration of 70%, let stand overnight, took the supernatant, concentrated under reduced pressure, removed ethanol, added water Dilute to 1000mL to get the traditional Chinese medicine Zhenlian Zengjian Oral Liquid;

[0056] Among them, Ligustrum lucidum, Eclipta chinensis, Epimedium, Astragalus, Burdock and Gynostemma were all purchased from the Anguo medicinal material market, and all met the 2015 (Ⅱ) regulations of "The Veterinary Pharmacopoeia of the People's Republic of China";

[0057] Get the Chinese medicine Zhenlian Zengmian Oral Liquid of Example 1 as the test drug, and take the mice w...

Embodiment 2

[0059] The quality detection of embodiment 2 Chinese medicine Zhenlian Zengjian Oral Liquid

[0060] 1) Preparation of Ecliptasin A Reference Substance Solution

[0061] Add an appropriate amount of Eclipta glucoside A reference substance, add methanol to make a solution containing 0.5mg per 1mL, and use it as the Eclipta chinensis reference substance solution.

[0062] 2) Preparation of Eclipta chinensis reference medicinal material solution

[0063]Add 25 mL of 70% methanol to ultrasonic treatment for 45 minutes, let cool, filter, and recover the solvent from the filtrate to dryness, add 25 mL of water to the residue to dissolve, shake and extract twice with chloroform, 20 mL each time, discard Remove the chloroform solution, shake the water solution with ethyl acetate twice, 20 mL each time, combine the ethyl acetate solution, recover the solvent to dryness, add 1 mL of ethyl acetate to the residue to dissolve, and use it as the Eclipta chinensis reference medicinal materi...

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Abstract

The invention discloses a quality control method of traditional Chinese medicine Zhenlian immunity-boosting oral solution. The Zhenlian immunity-boosting oral solution is prepared from six traditionalChinese medicines: fructus ligustri lucidi, eclipta, herba epimedii, astragalus membranaceus, great burdock achene and synostemma pentaphylla; the detection method is simple in operation, the ecliptaand the herba epimedii in the traditional Chinese medicine Zhenlian immunity-boosting oral solution can be authenticated by adopting a thin-layer chromatography, nuezhenide and icariin in the traditional Chinese medicine Zhenlian immunity-boosting oral solution can be simultaneously detected by adopting the high-performance liquid chromatography, thereby effectively performing quality analysis onthe traditional Chinese medicine Zhenlian immunity-boosting oral solution, and reflecting the quality status of the traditional Chinese medicine Zhenlian immunity-boosting oral solution more comprehensively; the quality level of the product is improved, and the quality stability of the product is guaranteed. Furthermore, the quality detection method of the traditional Chinese medicine Zhenlian immunity-boosting oral solution is good in specificity, repeatability and accuracy, and can be used for performing comprehensive assessment on the quality of the traditional Chinese medicine Zhenlian immunity-boosting oral solution, thereby effectively controlling the quality of the traditional Chinese medicine Zhenlian immunity-boosting oral solution and guaranteeing the clinical use security, theeffectiveness and the stability.

Description

technical field [0001] The invention belongs to the field of veterinary medicine, and relates to the field of quality detection of a compound traditional Chinese medicine for enhancing the immunity of livestock and poultry, in particular to a quality detection method of the traditional Chinese medicine Zhenlian Zengjian Oral Liquid. Background technique [0002] With the continuous development and intensification of the poultry breeding industry, the growth environment of poultry and livestock has been continuously improved, and the production performance has been maximized. At the same time, activities have been restricted. Self-regulation function declines, resistance is poor, and many factors in breeding management, such as weather changes, water and electricity cuts, replacement of breeders, vaccine immunization, etc., may become the cause of its disease. In order to prevent and control diseases, the traditional method is to use a large amount of antibiotics. As a result...

Claims

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Application Information

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IPC IPC(8): G01N30/90G01N30/06G01N30/02
CPCG01N30/02G01N30/06G01N30/90G01N2030/027
Inventor 陆安杜红娜刘炳伟郭宽郭永国贾永兵郭永红
Owner SHIJIAZHUANG WEIERLI ANIMAL PHARMA
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