Biaxially-oriented polyester film with high compound fastness for TTR (thermal transfer ribbon) and preparation method of biaxially-oriented polyester film
A technology of biaxially oriented polyester and compound fastness, applied in the field of polyester film, can solve the problems of low adhesion of polyester film ink, film holes, printing loss, etc., and achieve high ink compound fastness and ink adhesion. The effect of improving and increasing the crystallization rate
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Embodiment 1
[0033] A kind of preparation method of biaxially stretched polyester film for carbon tape with high composite fastness, it may further comprise the steps:
[0034] A. Add 2%wt silane coupling agent to 93%wt toluene, prepare a solution, add 5%wt silica with a particle size of 1.5um, and disperse evenly in a high-speed disperser to obtain modified silica Silicon solution;
[0035] B. Add the modified silica solution to ethylene glycol and terephthalic acid, undergo semi-continuous esterification, polycondensation and drying to make PET polyester masterbatch, and make the content of silica particles 50000ppm ;
[0036] C. Dry the PET polyester chips in a fluidized bed at 140°C for 6 hours; add the dried PET polyester chips into the main extruder to heat and melt, and filter through a 15 μm disc filter to make the moisture content ≤ 50ppm;
[0037] Add 70wt% of PET polyester masterbatch and 30wt% of PET polyester chips into the auxiliary extruder to heat and melt, and separate t...
Embodiment 2
[0043] A kind of preparation method of biaxially stretched polyester film for carbon tape with high composite fastness, it may further comprise the steps:
[0044]A. Add 5%wt silane coupling agent to 89%wt toluene, prepare a solution, add 6%wt silica with a particle size of 2.0um, and disperse evenly in a high-speed disperser to obtain modified silica Silicon solution;
[0045] B. Add the silica solution modified by the silane coupling agent to ethylene glycol and terephthalic acid, and make PET polyester masterbatch through semi-continuous esterification, polycondensation and drying, and make the silica particles The content is 60000ppm;
[0046] C. Dry the PET polyester chips in a fluidized bed at 150°C for 5 hours; add the dried PET polyester chips into the main extruder to heat and melt, and filter through a 15 μm disc filter to make the moisture content ≤ 50ppm;
[0047] Add 75wt% of PET polyester masterbatch and 25wt% of PET polyester chips into an auxiliary extruder t...
Embodiment 3
[0053] A kind of preparation method of biaxially stretched polyester film for carbon tape with high composite fastness, it may further comprise the steps:
[0054] A. Add 4%wt silane coupling agent to 90%wt toluene, add 6%wt calcium carbonate with a particle size of 1.8um after preparing a solution, and disperse evenly in a high-speed disperser to obtain a modified calcium carbonate solution ;
[0055] B, the modified calcium carbonate solution is added in ethylene glycol and terephthalic acid, through semi-continuous esterification, polycondensation and drying to make PET polyester masterbatch, and the content of calcium carbonate particles is 55000ppm;
[0056] C. Dry the PET polyester chips in a fluidized bed at 160°C for 6 hours; add the dried PET polyester chips into the main extruder to heat and melt, and filter through a 15 μm disc filter to make the moisture content ≤ 50ppm;
[0057] Add 65wt% of PET polyester masterbatch and 35wt% of PET polyester chips into the auxi...
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