Preparation method of nanometer starch deodorant
A nano-starch and deodorant technology, applied in deodorization, disinfection and other directions, can solve the problems of complex process, corrosion, secondary pollution, etc., and achieve the effect of wide source of raw materials, simple procedure and mild conditions
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specific Embodiment approach 1
[0029] A preparation method of nano starch deodorant, comprising the steps of:
[0030] (1) Take an appropriate amount of corn starch and add it to a phosphate buffer solution with a pH of 5.0, wherein the concentration of the starch in the buffer solution is 10%, heat and stir in a boiling water bath for 50 minutes, fully gelatinize, and obtain a starch solution;
[0031] (2) Naturally cool the gelatinized starch solution to 58°C, add pullulanase solution according to the amount of 30 ASPU / g starch; then place it in a constant temperature water bath at 58°C for 8 hours; heat at 100°C for 50 minutes , to terminate the enzyme activity to obtain product A;
[0032] (3) Centrifuge the product A at 3000 rpm / min for 15 minutes; absorb the supernatant, store it in a refrigerator at 4°C for 12 hours for recrystallization; keep the temperature low, filter and wash 5 times, and dry in vacuum to obtain nano starch granules;
[0033] (4) Ultrasonic washing of the obtained nano-starch gr...
specific Embodiment approach 2
[0035] A preparation method of nano starch deodorant, comprising the steps of:
[0036] (1) Take an appropriate amount of cornstarch and add it into a citrate buffer solution with pH=5.0, wherein the concentration of the starch in the buffer solution is 5%, heat and stir in a boiling water bath for 30 minutes, fully gelatinize, and obtain a starch solution;
[0037] (2) Naturally cool the starch solution after gelatinization to 58°C, add pullulanase solution according to the amount of 30ASPU / g starch; then place it in a constant temperature water bath at 58°C for enzymolysis for 6h; heat at 100°C for 30 minutes , to terminate the enzyme activity to obtain product A;
[0038] (3) Centrifuge the product A at 3000 rpm / min for 15 minutes; absorb the supernatant, store it in a refrigerator at 4°C for 12 hours for recrystallization; keep the temperature low, filter and wash 5 times, and dry in vacuum to obtain nano starch granules;
[0039] (4) Ultrasonic washing of the obtained na...
specific Embodiment approach 3
[0041] A preparation method of nano starch deodorant, comprising the steps of:
[0042] (3) adding an appropriate amount of potato starch into a phosphate buffer solution with pH=6.0, wherein the concentration of the starch in the buffer solution is 10%, heating and stirring in a boiling water bath for 50 minutes, fully gelatinizing, and obtaining a starch solution;
[0043] (4) Naturally cool the gelatinized starch solution to 58°C, add pullulanase solution according to the amount of 30 ASPU / g starch; then place it in a constant temperature water bath at 58°C for 12 hours; heat at 100°C for 50 minutes , to terminate the enzyme activity to obtain product A;
[0044] (3) Centrifuge the product A at 3000 rpm / min for 15 minutes; absorb the supernatant, store it in a refrigerator at 4°C for 12 hours for recrystallization; keep the temperature low, filter and wash 5 times, and dry in vacuum to obtain nano starch granules;
[0045] (4) Ultrasonic washing of the obtained nano-starch...
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