Toothpaste containing polygonum cuspidatum and preparation method of toothpaste
A technology for toothpaste and knotweed, which is applied in the field of daily chemical products, can solve the problems of high polarity of solvents, reduced activity, and reduced bacteriostatic effect of antibacterial components, and achieves the conditions of mild preparation method, maintenance of bacteriostatic activity, and good bactericidal effect Effect
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Embodiment 1
[0041] The components and weight percentages of the toothpaste containing Polygonum cuspidatum are: 0.5% of Polygonum cuspidatum extract, 18% of frictional silica, 3% of thickened silica, 13% of glycerin, 52% of sorbitol liquid, carboxymethyl cellulose Sodium 1%, Sodium Lauryl Sulfate 1.5%, Sodium Saccharin 0.1%, Sodium Benzoate 0.2%, Menthol 0.3%, Citric Acid 0.2%, Deionized Water 10.2%. The weight of Polygonum cuspidatum extract is calculated as the medicinal material.
[0042] Preparation:
[0043] (1) get 0.5 parts by weight of Polygonum cuspidatum and make powder after drying at 60 DEG C, then use 5 parts by weight of 70wt% ethanol to percolate and extract, the percolation speed is 3ml / kg / min, and the extract is dried to an extract sample, that is, the extract of Polygonum cuspidatum is obtained. thing;
[0044] (2) Add 0.5 parts by weight of deionized water to the Polygonum cuspidatum extract to dissolve, and centrifuge at 1500 r / min for 15 min to obtain a clear aqueous ...
Embodiment 2
[0050] The components and weight percentages of the toothpaste containing Polygonum cuspidatum are: 1% Polygonum cuspidatum extract, 18% frictional silica, 7% thickening silica, 15% glycerin, 46% sorbitol liquid, carboxymethyl cellulose Sodium 2%, Sodium Lauryl Sulfate 3%, Sodium Saccharin 0.3%, Sodium Benzoate 0.4%, Menthol 0.4%, Citric Acid 0.3%, Deionized Water 6.6%. The weight of Polygonum cuspidatum extract is calculated as the medicinal material.
[0051] Preparation:
[0052] (1) take 1 part by weight of Polygonum cuspidatum and make powder after drying at 55 DEG C, then extract with 12 parts by weight of 70wt% ethanol, reflux at 80 DEG C for 45min, and dry the extract to an extract sample to obtain the Polygonum cuspidatum extract;
[0053] (2) Polygonum cuspidatum extract is dissolved in 3 parts by weight of deionized water, and filtered to obtain a clear aqueous solution of Polygonum cuspidatum extract;
[0054] (3) add 0.4 parts by weight of sodium benzoate, 0.3 p...
Embodiment 3
[0059] The components and weight percentages of the toothpaste containing Polygonum cuspidatum are: 4% of Polygonum cuspidatum extract, 25% of frictional silica, 6% of thickened silica, 10% of glycerin, 40% of sorbitol liquid, carboxymethyl cellulose Sodium 2.5%, Sodium Lauryl Sulfate 2.2%, Sodium Saccharin 0.5%, Sodium Benzoate 0.2%, Menthol 0.5%, Citric Acid 0.3%, Arginine 0.1%, Deionized Water 8.7%. The weight of Polygonum cuspidatum extract is calculated as the medicinal material.
[0060] Preparation:
[0061] (1) get 4 parts by weight of Polygonum cuspidatum and make powder after drying at 50 DEG C, then use 60 parts by weight of 80wt% ethanol to ultrasonically extract, ultrasonically 30min, and the extract is dried to an extract sample to obtain Polygonum cuspidatum extract;
[0062] (2) Polygonum cuspidatum extract is dissolved in 6 parts by weight of deionized water, and filtered with multi-layer gauze to obtain a clear aqueous solution of Polygonum cuspidatum extrac...
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