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Microemulsion type long-acting edible detergent and preparation method thereof

A microemulsion, detergent technology, applied in the direction of surface active detergent composition, detergent composition, detergent compounding agent, etc., can solve the problem of inability to formulate detergent, inability to store for a long time, no foaming and decontamination ability, etc. problem, to achieve the effect of long-lasting, safe and non-toxic, avoiding hydrolysis degradation, and strong washing effect

Active Publication Date: 2019-03-12
NINGBO YUFANGTANG BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Compared with the requirements of the real edible detergent in terms of formula, dosage form and preparation process, the above-mentioned scheme still has many deficiencies, resulting in the failure of marketization of related liquid and jelly products that are convenient to use, and its restrictive bottlenecks focus on the following three point:
[0010] ①Classic food-grade products with wetting, dispersing, emulsifying and washing functions, mostly non-ionic surfactants, tween, sucrose fatty acid esters, citric acid esters and polyglycerin fatty acid esters, HLB value Less than 16, the cleaning ability is extremely poor, and it is impossible to prepare detergent
However, food-grade glycyrrhizinate, ginsenoside and soybean saponin are expensive and difficult to commercialize;
[0011] ②Food-grade sodium fatty lactylate (such as sodium lauroyl lactylate), which has been successfully developed in recent years, has excellent decontamination and washing performance, and its degreasing effect is close to that of sodium dodecylbenzene sulfonate, but its hydrolysis resistance is poor, and the prepared water After one week, the agent has been hydrolyzed into a large amount of fatty acid salt, which not only affects the foam, consistency and cleaning effects, but also automatically withdraws from the food grade category because of the fatty acid salt soap, even solid powder will decompose and reduce efficacy due to moisture absorption , cannot be stored for a long time;
[0012] ③ It is difficult to thicken the classic food-grade surfactant products, and it is impossible to match the liquid and jelly products that meet the basic sensory requirements of consumers;
[0013] ④ The tableware cleaning powder mentioned in the patent application number CN201410329978.2 contains a large amount of non-food raw and auxiliary materials, which is easy to hurt hands after long-term use, and the detergency of sodium stearoyl lactylate decreases after absorbing moisture, so it is difficult to commercialize;
[0014] ⑤The vitamin E nano-microemulsion mentioned in patent application number CN201410477268.4, although it is a microemulsion, only has dispersion and emulsification, no foaming and decontamination capabilities, and does not belong to the category of edible detergents

Method used

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  • Microemulsion type long-acting edible detergent and preparation method thereof
  • Microemulsion type long-acting edible detergent and preparation method thereof
  • Microemulsion type long-acting edible detergent and preparation method thereof

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Experimental program
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Embodiment 1

[0038] The microemulsion type long-acting edible detergent of the present embodiment is a kind of edible detergent, comprises following weight component:

[0039]

[0040] The preparation method of above-mentioned microemulsion type long-acting edible detergent comprises the following steps:

[0041] (1) Pre-ingredients

[0042] Under stirring conditions, add food-grade sodium lauroyl lactylate and food-grade food-grade decaglycerol monolaurate into water heated to 50-60°C according to the formula amount, stir for 30 minutes until completely transparent, add food Grade phytic acid and food grade sodium phytate, temperature controlled at 50-60°C, stirred for 20 minutes until completely transparent, to obtain phase A material;

[0043] Heat food-grade food-grade caprylic monoglyceride to 50-60°C, stir for 20 minutes until it becomes a completely mixed liquid, and obtain the B-phase material;

[0044] (2) Microemulsion modulation

[0045] Put the material of phase A into th...

Embodiment 2

[0049] The microemulsion type long-acting edible detergent of the present embodiment is a kind of edible hand sanitizer, comprises following weight component:

[0050]

[0051]

[0052] Edible hand sanitizer preparation method comprises the following steps in the present embodiment:

[0053] (1) Pre-ingredients

[0054] Under stirring conditions, food grade sodium lauroyl lactylate, food grade sodium stearoyl lactylate, food grade food grade decaglyceryl monolaurate and food grade decaglycerol monocaprylate were added to the Add food-grade phytic acid and food-grade sodium phytate to water that has been heated to 50-60°C, control the temperature at 50-60°C, stir for 20 minutes until completely transparent, and obtain the A-phase material;

[0055] Heat food-grade caprylic acid monoglyceride to 50-60°C, stir for 20 minutes until it becomes a completely mixed liquid, and obtain phase B material;

[0056] (2) Microemulsion modulation

[0057] Put the material of phase A ...

Embodiment 3

[0061] The microemulsion type long-acting edible detergent of the present embodiment is a kind of edible shampoo jelly, comprises following component:

[0062]

[0063] The preparation method of edible shampoo jelly in the present embodiment comprises the following steps:

[0064] (1) Pre-ingredients

[0065] Under stirring conditions, add food-grade sodium lauroyl lactylate and food-grade food-grade decaglycerol monolaurate into water heated to 50-60°C according to the formula amount, stir until completely transparent, add food-grade phytic acid With food-grade sodium phytate, control the temperature at 50-60°C, stir for 20 minutes until completely transparent, and obtain the A-phase material;

[0066] Heat food-grade food-grade caprylic monoglyceride to 50-60°C, stir until it becomes a completely mixed liquid, and obtain the B-phase material;

[0067] (2) Microemulsion modulation

[0068] Put the material of phase A into the micro-emulsion pot, strictly control the tem...

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Abstract

The invention relates to a microemulsion type long-acting edible detergent and a preparation method thereof. The present discloses a microemulsion system capable of enabling fatty lactolactate sodiumto be stabilized in a water phase for a long time; the ester group in the fatty lactolactate sodium is effectively protected by using a unique molecular structure of polyglycerol, mainly containing straight chains and trace loop chains, in decapol mono-fatty acid ester and the lipophilic affinity of the medium-chain fatty acid monoglyceride, and the advantages of strong detergent washing, efficient bubbling and the like of the fatty lactolactate sodium are exerted to the maximum extent, so that a finished product can be stored for over 200 days; in addition, by ingenious use of the thickeningprinciple of a high-oil-phase emulsion a high-denseness O / W microemulsion transparent system with refreshing skin feeling is prepared, which avoids the bubble suppression shortcoming of a lipid substance; the prepared edible detergent has a desirable density, uniform texture and strong washing effect, can preserve the moisture and protect the skin, is obvious in bubbling and has a long-lasting effect; meanwhile, edible body lotion disclosed by the invention is safe and nontoxic; and occasional ingestion is not harmful to health.

Description

technical field [0001] The invention relates to a microemulsion type long-acting edible detergent and a preparation method thereof. Background technique [0002] Modern cleaning and care products composed of surfactants (such as detergent, shower gel, shampoo, hand sanitizer, facial cleanser and laundry detergent, etc.) are difficult for consumers to rinse with water after use due to the adsorption effect in surface chemistry. Many health hazards caused by trace amounts of synthetic chemical raw materials remaining on the skin surface have aroused the vigilance of the whole society. The new era of green environmental protection concept calls for the market of edible detergents composed of food-grade raw materials. To this end, the industry has poured a lot of effort into the development of such products, as detailed below: [0003] 1. Patent application number 201310076181.1, authorized announcement number CN103113997B's Chinese patent "A Food-grade Detergent and Its Prepar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/55A61K8/39A61K8/37A61K8/06A61Q5/02A61Q19/10A61Q19/00C11D1/83C11D3/60C11D3/36C11D3/382C11D3/50
CPCA61K8/068A61K8/37A61K8/375A61K8/39A61K8/553A61K2800/30A61Q5/02A61Q19/00A61Q19/10C11D1/04C11D1/667C11D1/74C11D1/83C11D3/362C11D3/382C11D3/50
Inventor 贾福怀马云龙许璐云杨卫平袁媛王彩霞戴飞熊菲菲
Owner NINGBO YUFANGTANG BIOTECH