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Thermal-stability high-impact-resistance polycrystalline diamond compact and preparing method thereof

A technology of diamond composite sheet and polycrystalline diamond, which is applied in metal processing equipment, transportation and packaging, etc., can solve the problems of reducing the thermal stability and wear resistance of polycrystalline diamond layer, failure of polycrystalline diamond layer composite sheet, etc., to achieve Reduce the harmful residual stress of the interface, improve the impact resistance and collapse resistance, and improve the drilling efficiency

Active Publication Date: 2019-03-29
KINGDREAM PLC CO +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But at the same time, a higher cobalt content will reduce the thermal stability and wear resistance of the polycrystalline diamond layer, because the large difference in thermal expansion coefficient between cobalt and diamond will cause microcracks between the bonds of diamond grains under heated conditions, resulting in fragmentation of the polycrystalline diamond layer and early failure of the compact

Method used

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  • Thermal-stability high-impact-resistance polycrystalline diamond compact and preparing method thereof
  • Thermal-stability high-impact-resistance polycrystalline diamond compact and preparing method thereof
  • Thermal-stability high-impact-resistance polycrystalline diamond compact and preparing method thereof

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preparation example Construction

[0040] The steps of the preparation method of the heat-stable high impact-resistant polycrystalline diamond composite sheet proposed by the present invention are as follows:

[0041] The first step is to mix double-layer diamond powder with different particle sizes;

[0042] In the second step, the mixed double-layer diamond powder, the cemented carbide substrate 200 with a parallel groove-like interface, and various assembly components are assembled internally and externally to form an external composite mold (internal assembly refers to the use of metal materials) The cup wraps the cemented carbide matrix 200 and diamond powder, and the small parts formed are called the inner composite mold; the outer assembly refers to wrapping the inner composite mold with various salt parts and pyrophyllite blocks, and the small parts formed are called the outer composite mold. );

[0043] The third step is to put the outer synthetic mold into the six-sided top press, and sinter it into a ...

Embodiment 1

[0068] This embodiment is a thermally stable high-impact polycrystalline diamond composite sheet with a diameter of 15.88 mm and a height of 13.22 mm. First, mix the diamond powder of the surface layer and the transition layer: the main particle size of the surface layer powder is 10-20mm, and the main particle size of the transition layer powder is 25-35mm. The mixed double-layer powder is fired at 650-750° C. for 30-90 minutes in a hydrogen atmosphere. Put the fired double-layer powder into the metal cup sequentially according to the ratio of the thickness of the surface layer to 1.0mm and the thickness of the transition layer to 1.5mm, and the cemented carbide substrate with parallel groove interface, and perform internal assembly to obtain the internal composite mold. The inner synthetic mold is subjected to heat treatment at 500-1200° C. for 90-150 minutes in an argon atmosphere. Externally assemble the heat-treated inner composite mold with other assembly components to ...

Embodiment 2

[0074] This embodiment is a thermally stable high-impact polycrystalline diamond composite sheet with a diameter of 15.88 mm and a height of 13.22 mm. First, mix the diamond powder of the surface layer and the transition layer: the main particle size of the surface layer powder is 15-25mm, and the main particle size of the transition layer powder is 35-45mm. The mixed double-layer powder is fired at 650-750° C. for 30-90 minutes in a hydrogen atmosphere. Put the fired double-layer powder into the metal cup sequentially according to the ratio of surface layer thickness of 1.0mm and transition layer thickness of 2.0mm, and cemented carbide substrate with parallel groove interface, and perform internal assembly to obtain an internal composite mold. The inner synthetic mold is subjected to heat treatment at 500-1200° C. for 90-150 minutes in an argon atmosphere. Externally assemble the heat-treated internal composite mold with other assembly components to obtain an external compo...

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Abstract

The invention discloses a thermal-stability high-impact-resistance polycrystalline diamond compact. The thermal-stability high-impact-resistance polycrystalline diamond compact comprises a hard alloymatrix and a polycrystalline diamond layer; the polycrystalline diamond layer comprises a transition layer close to one side of the hard alloy matrix and a surface layer away from one side of the hardalloy matrix; the surface layer and the transition layer of the polycrystalline diamond layer are prepared through multi-granularity diamond powder ingredients, the main granularity of the surface layer powder ranges from 5 micrometers to 25 micrometers, the main granularity of the transition layer powder ranges from 25 micrometers to 45 micrometers, and the thickness ratio of the surface layer to the transition layer is 1:1-1:3. According to the thermal-stability high-impact-resistance polycrystalline diamond compact, drilling efficiency can be improved, the drilling period can be shortened,the service life is prolonged, and the drilling cost is effectively reduced.

Description

technical field [0001] The invention relates to the technical field of superhard materials, in particular to a heat-stable high-impact polycrystalline diamond composite sheet and a preparation method thereof. Background technique [0002] Polycrystalline diamond compact (PDC) generally consists of two layers of material - the upper layer of polycrystalline diamond layer and the lower layer of cemented carbide substrate. Generally, it is made of diamond powder and cemented carbide matrix by sintering and compounding under high temperature and high pressure (HTHP). Diamond composite sheet has both the high wear resistance of the diamond layer and the high toughness of the cemented carbide matrix, and is a very important cutting element for oil and gas drilling tools. [0003] With the continuous development of the oil and gas development industry and the development of unconventional energy such as shale gas and shale oil, the production conditions and requirements for drilli...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F1/00B22F3/14B22F7/04B22F3/24C22C26/00
CPCC22C26/00B22F3/14B22F3/24B22F7/04B22F2003/241B22F1/052
Inventor 田红平陈文婷徐磊张烈华刘洋
Owner KINGDREAM PLC CO