Femtosecond laser instant color development and regulation method
A femtosecond laser, reddish-brown technology, applied in the field of glass color development, can solve the problems of difficult to maintain chemical stability, color development is difficult to maintain for a long time, complex preparation process, etc., to achieve considerable application prospects, wide range of glass formation, The effect of simple process
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Embodiment 1
[0033] Select silicon dioxide, boric acid, lead oxide, bismuth trioxide and antimony trioxide as starting compound raw materials, and weigh five compound raw materials respectively according to the molar ratio of each element, and the proportions are as follows:
[0034] B:Pb:Si:Bi:Sb=108:15:11:36:4, corresponding to x=58, y=15, z=11;
[0035] The total weight of the control mixture is 60g. After grinding and mixing 60g of the mixture, put it into a corundum crucible, then put the crucible into a muffle furnace at a temperature of 500°C, pretreat for 60 minutes, and then transfer the crucible to a high-temperature electric furnace at 1200°C.
[0036] The samples were melted at 1200 °C for 30 min. Take out the corundum crucible at high temperature, and quickly pour the melt on a stainless steel plate at room temperature. In order to accelerate cooling, press quickly with another stainless steel plate to obtain the required sample, and select the appropriate size of the sample ...
Embodiment 2
[0040] Select silicon dioxide, boric acid, lead oxide, bismuth trioxide and antimony trioxide as starting compound raw materials, weigh five compound raw materials respectively according to the molar ratio of each element, and divide them into four groups of ingredients, and four groups of ingredients For example:
[0041] (1) B:Pb:Si:Bi:Sb=132:0:14:36:4, corresponding to x=66, y=0, z=14;
[0042] (2) B:Pb:Si:Bi:Sb=116:10:12:36:4, corresponding to x=58, y=10, z=12;
[0043] (3) B:Pb:Si:Bi:Sb=100:20:10:36:4, corresponding to x=50, y=20, z=20;
[0044] (4) B:Pb:Si:Bi:Sb=82:30:9:36:4, corresponding to x=41, y=30, z=9;
[0045] The mixture gross weight of control four groups is 60g.
[0046] After each group of 60g mixture was ground and mixed, it was put into a corundum crucible, and then the crucible was placed in a muffle furnace at a temperature of 500°C for pretreatment for 60 minutes, and then the crucible was transferred to a high-temperature electric furnace at a temperat...
Embodiment 3
[0049] Select silicon dioxide, boric acid, lead oxide, bismuth trioxide and antimony trioxide as starting compound raw materials, and weigh five compound raw materials respectively according to the molar ratio of each element, and the proportions are as follows:
[0050] B:Pb:Si:Bi:Sb=132:0:14:36:4, corresponding to x=66, y=0, z=14;
[0051] The total weight of the control mixture is 60g. After grinding and mixing 60g of the mixture, put it into a corundum crucible, then put the crucible into a muffle furnace at a temperature of 400°C, pretreat for 2 hours, and then transfer the crucible to a high-temperature electric furnace at 1250°C. The sample was melted at 1250 °C for 60 min. Take out the corundum crucible at high temperature, and quickly pour the melt on a stainless steel plate at room temperature. In order to accelerate cooling, press quickly with another stainless steel plate to obtain the required sample, and select the appropriate size of the sample for cutting, gri...
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