A kind of water-based electronic slurry and preparation method thereof
An electronic paste, water-based technology, applied in the direction of cable/conductor manufacturing, conductive materials dispersed in non-conductive inorganic materials, circuits, etc., can solve the problems of adverse effects of electronic paste performance, high production cost, complicated methods, etc. , to achieve the effects of easy promotion, green environmental protection cost, and simple preparation process
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[0021] The preparation method of water-based electronic slurry of the present invention is implemented according to the following steps:
[0022] Preparatory step: Weigh the following components according to mass percentage: 1% to 10% of nano-organic bentonite, 60% to 80% of conductive phase, 1% to 5% of conductive enhancement phase, 5% to 15% of lead-free glass powder, polar Activator 1%-5%, auxiliary suspending agent carboxymethyl cellulose 0.2%-2.0%, polyacrylamide 0.05%-0.5%, deionized water 15%-30%, total 100%;
[0023] Step 1: preparing nano-organic bentonite gel,
[0024] Adding methanol with a mass concentration of 95% to the nano-organic bentonite, mixing evenly, placing it under a high-speed mixer and stirring for 5-15 minutes to prepare a nano-organic bentonite gel, sealing it for 10-30 hours for use;
[0025] Step 2: Prepare metal composite powder conductive phase,
[0026] Mix copper powder, silver powder and nickel powder with a particle size of 1-10 μm evenly,...
Embodiment 1
[0032] Preparatory steps: Weigh the following components according to mass percentage: nano-organic bentonite 5%, conductive phase silver powder, copper powder and nickel powder 62% in total, conductive enhancement phase graphene nanosheet 3%, low melting point ZnO-B 2 o 3 -Si0 2 10% glass powder, 3% methanol with a mass concentration of 95%, 1.5% carboxymethylcellulose as an auxiliary suspending agent, 0.5% polyacrylamide, 15% deionized water, the total is 100%;
[0033] Step 1: preparing nano-organic bentonite gel,
[0034] Add methanol with a mass concentration of 95% into the nano-organic bentonite, mix evenly, place it under a high-speed mixer and stir for 10 minutes to prepare a nano-organic bentonite gel, and seal it for 24 hours for use;
[0035] Step 2: Prepare metal composite powder conductive phase,
[0036] Mix copper powder, silver powder and nickel powder with a particle size of 5 μm evenly, and pickle the metal powder with dilute sulfuric acid with a mass fra...
Embodiment 2
[0040]Preparatory steps: Weigh the following components according to mass percentage: nano-organic bentonite 5%, conductive phase silver powder, copper powder and nickel powder 60% in total, conductive enhancement phase graphene nanosheet 3%, low melting point ZnO-B 2 o 3 -Si0 2 10% glass powder, 5% methanol with a mass concentration of 95%, 1.5% carboxymethylcellulose as an auxiliary suspending agent, 0.5% polyacrylamide, 15% deionized water, the total is 100%;
[0041] Step 1: preparing nano-organic bentonite gel,
[0042] Add methanol with a mass concentration of 95% into the nano-organic bentonite, mix evenly, place it under a high-speed mixer and stir for 10 minutes to prepare the nano-organic bentonite gel, and seal it for 24 hours for use.
[0043] Step 2: Prepare metal composite powder conductive phase,
[0044] Copper powder, silver powder and nickel powder with a particle size of 3 μm are evenly mixed, and then the metal powder is pickled with dilute sulfuric acid...
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