Organic-inorganic composite silicate high-temperature-resistant film-forming drilling fluid system
A composite silicate and organosilicate technology, applied in the field of drilling fluid, to achieve the effects of good film quality, good filtration loss reduction, and good plugging performance
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Embodiment 1
[0035] Example 1: The organic-inorganic composite silicate high temperature film-forming drilling fluid system of this example contains methyl silicate with a concentration of 0.2 mol / L and silicate C with a concentration of 0.06 mol / L, and is prepared by the following steps. Obtained: Add the weighed methyl silicate and silicate C to 300 mL of distilled water, stir magnetically for 20 min, put them into a high-temperature reaction kettle with 40 g of cuttings, react at 180 °C for 16 h, and dry After treatment, weigh the mass and observe the film formation on the cuttings surface. See details for details. figure 1 .
Embodiment 2
[0036] Example 2: The organic-inorganic composite silicate high temperature film-forming drilling fluid system of this example, containing 2% organic silane and 1% silicate D by mass fraction, was prepared by the following steps: Add the weighed organosilane and silicate D to 300mL of distilled water, stir magnetically for 20min, put it into a high-temperature reaction kettle with 40g of cuttings, react at 180°C for 16h, and weigh the mass after drying. , and observe the film formation phenomenon on the surface of cuttings, see details figure 2 .
Embodiment 3
[0037] Example 3: The organic-inorganic composite silicate high temperature film-forming drilling fluid system of this example contains methyl silicate with a concentration of 0.2 mol / L and silicate C with a concentration of 0.06 mol / L, and is prepared by the following steps. Obtained: Add the weighed methyl silicate A and silicate C into 300 mL of distilled water, stir magnetically for 20 min, put them into a high-temperature reaction kettle with 40 g of cuttings, react at 220 °C for 16 h, and bake After dry treatment, weigh the mass and observe the film formation on the surface of the cuttings. For details, see image 3 .
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