Method for preparing perilla peptide
The technology of perilla peptide and perilla meal is applied in the field of preparation of perilla peptide, which can solve the problems of waste of resources and low utilization rate of nutrients, and achieve the effects of reducing waste, being easy to absorb, and improving utilization rate.
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[0015] The embodiment of the present invention provides a preparation method of perilla peptide, comprising the following steps:
[0016] (1) After the pulverized perilla meal is subjected to denaturation treatment, the perilla meal protein liquid is obtained;
[0017] (2) The perilla meal protein solution in step (1) is enzymolyzed by α-amylase, alkaline protease and compound protease in sequence to obtain an enzymatic hydrolysis product;
[0018] (3) The enzymatic hydrolysis product in step (2) is subjected to enzyme inactivation, decolorization, concentration and freeze-drying to obtain a finished product.
[0019] In the present invention, the denaturation treatment of perilla meal adopts the following method: after mixing the pulverized perilla meal with water, heat it at 80-85°C for 1-2 hours, wherein the mass ratio of perilla meal to water is 1:15- 20.
[0020] In the present invention, the perilla meal is defatted perilla meal, and the defatted perilla meal is crushe...
Embodiment 1
[0034] Embodiment 1 of the present invention provides a kind of preparation method of perilla peptide, comprises the following steps:
[0035] (1) Grinding the defatted perilla meal until the particle size is less than 100um, mixing the obtained perilla meal powder with distilled water at a mass ratio of 1:18, and heating the mixture in a water bath at 82°C for 1 hour to obtain a perilla meal protein liquid;
[0036] (2) Adjust the pH of the perilla meal protein liquid in step (1) to 4.5, raise the temperature to 70° C., add α-amylase with a dry weight of perilla meal protein in an amount of 2 wt%, stir and mix evenly, and perform enzymatic hydrolysis for 2 hours , to obtain α-amylase hydrolysis product;
[0037] (3) Adjust the pH of the α-amylase hydrolyzate in step (2) to 8.5, and the temperature rises to 55° C., add Alcalase 2.4L alkaline protease with 2wt% dry weight of the α-amylase hydrolyzate, and stir After mixing evenly, enzymolyze for 3 hours to obtain alkaline prot...
Embodiment 2
[0041] Embodiment 2 of the present invention provides a kind of preparation method of perilla peptide, comprises the following steps:
[0042] (1) Crush the defatted perilla meal to a particle size of less than 100um, mix the obtained perilla meal powder with distilled water at a mass ratio of 1:15, and heat the mixture in a water bath at 80°C for 1.5 hours to obtain a perilla meal protein solution ;
[0043] (2) Adjust the pH of the perilla meal protein solution to 4 in step (1), raise the temperature to 65° C., and add α-amylase with a dry weight of perilla meal protein of 2 wt%, stir and mix evenly, and enzymolyze 2.5 h, to obtain α-amylase hydrolysis product;
[0044] (3) The pH of the α-amylase hydrolyzate in step (2) is adjusted to 8, the temperature rises to 50° C., and Alcalase 2.4L alkaline protease with a dry weight of 1.5 wt% of the α-amylase hydrolyzate is added, After stirring and mixing evenly, enzymatic hydrolysis for 3 hours to obtain the hydrolyzate of alkal...
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