Efficient phase-change energy storage composite and preparation method thereof
A phase change energy storage and composite material technology, applied in the field of high-efficiency phase change energy storage composite materials and their preparation, can solve the problems of low thermal conductivity, high risk coefficient, low energy storage density, etc., achieve high phase change enthalpy, overcome the The effect of small thermal conductivity and low production cost
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Embodiment 1
[0024] The material of the disguised energy storage material of this embodiment contains the following components by weight: 30 parts by weight of sodium sulfite; 10 parts by weight of A151 vinyltriethoxysilane; 50 parts by weight of crystalline wax (molecular weight: 2000); 10 parts by weight of water Parts: 4 parts by weight of m-phenylenediamine; 0.5 parts by weight of dibenzoyl peroxide; 0.5 parts by weight of dibutyltin diacetate.
[0025] Preparation method: 50 parts by weight of crystalline wax (molecular weight 2000), 10 parts by weight of hardener A151 vinyl triethoxysilane, 0.5 parts by weight of graft initiator DCP dibenzoyl peroxide, graft catalyst diacetate diacetate Mix under the action of 0.5 parts by weight of butyltin, and mix at 90° C. for 6 hours under ultraviolet light irradiation to prepare a crystalline wax prepolymer. Then, the formed crystalline wax prepolymer was mixed with 30 parts by weight of sodium sulfite (10 parts of water) at 120°C in a high-spe...
Embodiment 2
[0027] The material of the disguised energy storage material of this embodiment contains the following components by weight: 40 parts by weight of sodium sulfite; 5 parts by weight of hardener A171 vinyl trimethoxy silicon; 40 parts by weight of crystal wax (molecular weight: 3000); 15 parts by weight of water. Parts by weight; 3 parts by weight of diaminodiphenylmethane; 0.8 parts by weight of dibenzoyl peroxide; 0.8 parts by weight of dibutyltin diacetate.
[0028] Preparation method: 40 parts by weight of crystalline wax (molecular weight 3000), 5 parts by weight of hardener A171 vinyl trimethoxy silicon, 0.8 parts by weight of graft initiator DCP dibenzoyl peroxide, graft catalyst diacetate diacetate Mix under the action of 0.8 parts by weight of butyltin, and mix at 90° C. for 6 hours under ultraviolet light irradiation to prepare a crystalline wax prepolymer. Then the formed crystalline wax prepolymer was stirred and mixed with 40 parts by weight of sodium sulfite (15 pa...
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