Quality detection method for jujube kernel Anshen liquid

A quality inspection method, Zaoren Anshen technology, applied in measuring devices, instruments, scientific instruments, etc., can solve problems such as poor reliability and slow detection speed, and achieve the effect of ensuring stability

Inactive Publication Date: 2019-07-23
LIAONING XIANCAOTANG PHARMA
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  • Abstract
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Problems solved by technology

[0006] In view of this, the present invention provides a quality detection method of Zaoren Anshen Liquid,

Method used

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  • Quality detection method for jujube kernel Anshen liquid
  • Quality detection method for jujube kernel Anshen liquid
  • Quality detection method for jujube kernel Anshen liquid

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[0026] The present invention is further explained below in conjunction with specific embodiments, but it is not used to limit the protection scope of the present invention.

[0027] 1. Instruments and reagents

[0028] Shimadzu 20A high performance liquid chromatograph consists of LC-20AT quaternary pump, SPD-M20A diode array detector (DAD), SIL-20A autosampler and CTO-20A column oven. The reference substances Spinosin (batch number 111869-201704), salvianolic acid B (batch number 111562-201716), and schisandrin A (batch number 110857-201714) were all purchased from China Institute for Food and Drug Control. Both methanol and acetonitrile are chromatographically pure, water is double-distilled water, and other reagents are analytically pure.

[0029] 2. Chromatographic conditions and system suitability test

[0030] Chromatographic column: Agilent Zorbax Eclipse Plus C18 (250mm×4.6mm, 5μm); mobile phase: acetonitrile (A)-0.1% glacial acetic acid solution (B), gradient elution (0~16mi...

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Abstract

The invention discloses a quality detection method for jujube kernel Anshen liquid. The detection method adopts high performance liquid chromatography to measure the content of spinosin in the jujubekernel, the content of salvianolic acid B in radix salviae miltiorrhizae and the content of schisandrin in the fruit of Chinese magnoliavine in the jujube kernel Anshen liquid, the quality of the jujube kernel Anshen liquid can be comprehensively evaluated and controlled, so that a comprehensive and reliable basis is provided for the internal quality detection of the jujube kernel Anshen liquid, and the stability of product quality as well as the safety and the effectiveness of clinical medication can be guaranteed.

Description

technical field [0001] The invention discloses the technical field of quality control of traditional Chinese medicines, in particular to a quality detection method of Zaoren Anshen Liquid. Background technique [0002] Zaoren Anshen Liquid is now recorded in the 18th volume of traditional Chinese medicine preparations in the "Drug Standards of the Ministry of Health". The standard number is WS3-B-3429-98. Deficiency, neurasthenia caused by insomnia, forgetfulness, dizziness, headache embolism. In the prescription, Suanzaoren is used to nourish the heart and yin, nourish the liver and blood, and calm the heart and calm the nerves as the king drug; Salvia miltiorrhiza clears the heart and cools the blood, nourishes the blood and calms the nerves; The combination of the three medicines has the functions of invigorating the heart and nourishing the liver, calming the nerves and improving intelligence. [0003] The current standard quality control item is TLC method to identify...

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Application Information

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IPC IPC(8): G01N30/02G01N30/06
CPCG01N30/02G01N30/06G01N2030/027
Inventor 王安宁王南程小东张雅薇
Owner LIAONING XIANCAOTANG PHARMA
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